10-phenyl-2-(4-piperidyl)-5,10-dihydro-5λ⁶-benzo[e][1,2,4]triazolo-[1,5-b][1,2,4]thiadiazine-5,5-dione

Base Information

• Chemical Name: 10-phenyl-2-(4-piperidyl)-5,10-dihydro-5λ⁶-benzo[e][1,2,4]triazolo-[1,5-b][1,2,4]thiadiazine-5,5-dione
• CAS No.: 956609-23-7
• Molecular Formula: C₁₉H₁₉N₅O₂S
• Molecular Weight: 381.458

Synonyms:10-phenyl-2-(4-piperidyl)-5,10-dihydro-5λ⁶-benzo[e][1,2,4]triazolo-[1,5-b][1,2,4]thiadiazine-5,5-dione

Chemical Property of 10-phenyl-2-(4-piperidyl)-5,10-dihydro-5λ⁶-benzo[e][1,2,4]triazolo-[1,5-b][1,2,4]thiadiazine-5,5-dione

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Technology Process of 10-phenyl-2-(4-piperidyl)-5,10-dihydro-5λ⁶-benzo[e][1,2,4]triazolo-[1,5-b][1,2,4]thiadiazine-5,5-dione

There total 1 articles about 10-phenyl-2-(4-piperidyl)-5,10-dihydro-5λ⁶-benzo[e][1,2,4]triazolo-[1,5-b][1,2,4]thiadiazine-5,5-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

isonipecotic acid (498-94-2) + 3-hydrazino-4-phenyl-4H-1,2,4-benzothiadiazine 1,1-dioxide (107089-81-6) → 10-phenyl-2-(4-piperidyl)-5,10-dihydro-5λ6-benzo[e][1,2,4]triazolo-[1,5-b][1,2,4]thiadiazine-5,5-dione (956609-23-7)

Guidance literature:

With trichlorophosphate; Heating;

DOI:10.1016/j.bmcl.2007.07.043

Reference yield: 85.0%

10-phenyl-2-(4-piperidyl)-5,10-dihydro-5λ6-benzo[e][1,2,4]triazolo-[1,5-b][1,2,4]thiadiazine-5,5-dione (956609-23-7) + 2,4-Dichlorobenzenesulfonyl chloride (16271-33-3) → C25H21Cl2N5O4S2

Guidance literature:

With pyridine; at 20 ℃; for 4h;

DOI:10.1016/j.bmcl.2007.07.043

Reference yield: 70.0%

10-phenyl-2-(4-piperidyl)-5,10-dihydro-5λ6-benzo[e][1,2,4]triazolo-[1,5-b][1,2,4]thiadiazine-5,5-dione (956609-23-7) + 4-Fluorobenzenesulfonyl chloride (349-88-2) → C25H22FN5O4S2

Guidance literature:

With pyridine; at 20 ℃; for 4h;

DOI:10.1016/j.bmcl.2007.07.043

upstream raw materials:

isonipecotic acid

3-hydrazino-4-phenyl-4H-1,2,4-benzothiadiazine 1,1-dioxide

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