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Technology Process of N1-[1-(4'-chloro-4-biphenylyl)-2-(1-pyrrolidinyl)ethyl]-N2-(3,4-dichlorophenyl)-N1,N2-dimethylglycinamide

N1-[1-(4'-chloro-4-biphenylyl)-2-(1-pyrrolidinyl)ethyl]-N2-(3,4-dichlorophenyl)-N1,N2-dimethylglycinamide

Base Information
  • Chemical Name:N1-[1-(4'-chloro-4-biphenylyl)-2-(1-pyrrolidinyl)ethyl]-N2-(3,4-dichlorophenyl)-N1,N2-dimethylglycinamide
  • CAS No.:1003873-12-8
  • Molecular Formula:C28H30Cl3N3O
  • Molecular Weight:530.925
  • Hs Code.:
N<sub>1</sub>-[1-(4'-chloro-4-biphenylyl)-2-(1-pyrrolidinyl)ethyl]-N<sub>2</sub>-(3,4-dichlorophenyl)-N<sub>1</sub>,N<sub>2</sub>-dimethylglycinamide

Synonyms:N1-[1-(4'-chloro-4-biphenylyl)-2-(1-pyrrolidinyl)ethyl]-N2-(3,4-dichlorophenyl)-N1,N2-dimethylglycinamide

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Chemical Property of N1-[1-(4'-chloro-4-biphenylyl)-2-(1-pyrrolidinyl)ethyl]-N2-(3,4-dichlorophenyl)-N1,N2-dimethylglycinamide
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Technology Process of N1-[1-(4'-chloro-4-biphenylyl)-2-(1-pyrrolidinyl)ethyl]-N2-(3,4-dichlorophenyl)-N1,N2-dimethylglycinamide

There total 1 articles about N1-[1-(4'-chloro-4-biphenylyl)-2-(1-pyrrolidinyl)ethyl]-N2-(3,4-dichlorophenyl)-N1,N2-dimethylglycinamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

N<sub>1</sub>-[1-(4-bromophenyl)-2-(1-pyrrolidinyl)ethyl]-N<sub>2</sub>-(3,4-dichlorophenyl)-N<sub>1</sub>,N<sub>2</sub>-dimethylglycinamide
1003873-11-7

N1-[1-(4-bromophenyl)-2-(1-pyrrolidinyl)ethyl]-N2-(3,4-dichlorophenyl)-N1,N2-dimethylglycinamide

4-Chlorophenylboronic acid
1679-18-1

4-Chlorophenylboronic acid

N<sub>1</sub>-[1-(4'-chloro-4-biphenylyl)-2-(1-pyrrolidinyl)ethyl]-N<sub>2</sub>-(3,4-dichlorophenyl)-N<sub>1</sub>,N<sub>2</sub>-dimethylglycinamide
1003873-12-8

N1-[1-(4'-chloro-4-biphenylyl)-2-(1-pyrrolidinyl)ethyl]-N2-(3,4-dichlorophenyl)-N1,N2-dimethylglycinamide

Guidance literature:
With sodium carbonate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In 1,4-dioxane; water; at 185 ℃; for 0.1h; sealed glass reaction tube; microwave irradiation;
upstream raw materials:

N1-[1-(4-bromophenyl)-2-(1-pyrrolidinyl)ethyl]-N2-(3,4-dichlorophenyl)-N1,N2-dimethylglycinamide

4-Chlorophenylboronic acid

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