4-acetylaminophthalic acid diethyl ester

Base Information Edit

Chemical Name:4-acetylaminophthalic acid diethyl ester
CAS No.:149967-20-4
Molecular Formula:C₁₄H₁₇NO₅
Molecular Weight:279.293
Hs Code.:
Mol file:149967-20-4.mol

Synonyms:4-acetylaminophthalic acid diethyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-acetylaminophthalic acid diethyl ester Edit

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Technology Process of 4-acetylaminophthalic acid diethyl ester

There total 2 articles about 4-acetylaminophthalic acid diethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 22572-84-5
diethyl 4-aminophthalate

: 108-24-7
acetic anhydride

: 149967-20-4
4-acetylaminophthalic acid diethyl ester

Guidance literature:: With acetic acid; for 1h; Heating;
DOI:10.1021/jm060468y

Reference yield:

: 2050-19-3
4-nitrophthalic acid diethyl ester

: 149967-20-4
4-acetylaminophthalic acid diethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / FeCl₂; NaBH₄ / ethanol / 3 h / Heating

2: 87 percent / acetic acid / 1 h / Heating

With sodium tetrahydroborate; acetic acid; iron(II) chloride; In ethanol;
DOI:10.1021/jm060468y