3-O-Benzoyl-1,2-O-isopropyliden-5,6-di-O-methylsulfonyl-α-D-allofuranose

Base Information

• Chemical Name: 3-O-Benzoyl-1,2-O-isopropyliden-5,6-di-O-methylsulfonyl-α-D-allofuranose
• CAS No.: 31795-14-9
• Molecular Formula: C₁₈H₂₄O₁₁S₂
• Molecular Weight: 480.514

Synonyms:3-O-Benzoyl-1,2-O-isopropyliden-5,6-di-O-methylsulfonyl-α-D-allofuranose

Chemical Property of 3-O-Benzoyl-1,2-O-isopropyliden-5,6-di-O-methylsulfonyl-α-D-allofuranose

Chemical Property:

Purity/Quality:

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Technology Process of 3-O-Benzoyl-1,2-O-isopropyliden-5,6-di-O-methylsulfonyl-α-D-allofuranose

There total 7 articles about 3-O-Benzoyl-1,2-O-isopropyliden-5,6-di-O-methylsulfonyl-α-D-allofuranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

3-O-benzoyl-1,2-O-isopropylidene-α-D-allofuranose (31795-13-8) + methanesulfonyl chloride (124-63-0) → 3-O-Benzoyl-1,2-O-isopropyliden-5,6-di-O-methylsulfonyl-α-D-allofuranose (31795-14-9)

Guidance literature:

With pyridine; at 0 ℃; for 72h;

Reference yield:

benzoyl chloride (98-88-4) → 3-O-Benzoyl-1,2-O-isopropyliden-5,6-di-O-methylsulfonyl-α-D-allofuranose (31795-14-9)

Guidance literature:

Multi-step reaction with 3 steps

1: pyridine / CH₂Cl₂ / 1 h / 0 °C

2: aq. AcOH / 24 h / 20 °C

With pyridine; acetic acid; In dichloromethane;

DOI:10.1021/ja0360900

Reference yield:

Diacetone D-glucose (2595-05-3) → 3-O-Benzoyl-1,2-O-isopropyliden-5,6-di-O-methylsulfonyl-α-D-allofuranose (31795-14-9)

Guidance literature:

Multi-step reaction with 3 steps

1: pyridine / CH₂Cl₂ / 1 h / 0 °C

2: aq. AcOH / 24 h / 20 °C

With pyridine; acetic acid; In dichloromethane;

DOI:10.1021/ja0360900

upstream raw materials:

3-O-benzoyl-1,2-O-isopropylidene-α-D-allofuranose

methanesulfonyl chloride

(+)-3-deoxy-1,2:5,6-di-O-isopropylidene-α-D-allofuranos-3-yl benzoate

benzoyl chloride

Downstream raw materials:

3,6-di-O-benzoyl-1,2-O-isopropylidene-5-O-mesyl-α-D-allofuranose

3,5,6-tri-3-O-benzoyl-1,2-O-isopropylidene-β-L-talofuranose

Benzoic acid (3aR,5R,6R,6aR)-2,2-dimethyl-5-vinyl-tetrahydro-furo[2,3-d][1,3]dioxol-6-yl ester

3-O-benzoyloxy-5-deoxy-1,2-O-isopropylidene-α-D-ribohexofuranose

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