(2S,3S,4S,6S,7R,8S,9R,10R,13S,15R)-1-benzyloxy-8-tert-butyldimethylsilyloxy-3,6;10,13-bis-epoxy-15-[N-methyl-N-(toluene-4-sulfonyl)amino]-4-phenylseleno-2,7,9-trimethyloctadecane

Base Information

Chemical Name:(2S,3S,4S,6S,7R,8S,9R,10R,13S,15R)-1-benzyloxy-8-tert-butyldimethylsilyloxy-3,6;10,13-bis-epoxy-15-[N-methyl-N-(toluene-4-sulfonyl)amino]-4-phenylseleno-2,7,9-trimethyloctadecane
CAS No.:1415891-07-4
Molecular Formula:C₄₈H₇₃NO₆SSeSi
Molecular Weight:899.222
Hs Code.:

(2S,3S,4S,6S,7R,8S,9R,10R,13S,15R)-1-benzyloxy-8-tert-butyldimethylsilyloxy-3,6;10,13-bis-epoxy-15-[N-methyl-N-(toluene-4-sulfonyl)amino]-4-phenylseleno-2,7,9-trimethyloctadecane

Synonyms:(2S,3S,4S,6S,7R,8S,9R,10R,13S,15R)-1-benzyloxy-8-tert-butyldimethylsilyloxy-3,6;10,13-bis-epoxy-15-[N-methyl-N-(toluene-4-sulfonyl)amino]-4-phenylseleno-2,7,9-trimethyloctadecane

Suppliers and Price of (2S,3S,4S,6S,7R,8S,9R,10R,13S,15R)-1-benzyloxy-8-tert-butyldimethylsilyloxy-3,6;10,13-bis-epoxy-15-[N-methyl-N-(toluene-4-sulfonyl)amino]-4-phenylseleno-2,7,9-trimethyloctadecane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,3S,4S,6S,7R,8S,9R,10R,13S,15R)-1-benzyloxy-8-tert-butyldimethylsilyloxy-3,6;10,13-bis-epoxy-15-[N-methyl-N-(toluene-4-sulfonyl)amino]-4-phenylseleno-2,7,9-trimethyloctadecane

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of (2S,3S,4S,6S,7R,8S,9R,10R,13S,15R)-1-benzyloxy-8-tert-butyldimethylsilyloxy-3,6;10,13-bis-epoxy-15-[N-methyl-N-(toluene-4-sulfonyl)amino]-4-phenylseleno-2,7,9-trimethyloctadecane

There total 1 articles about (2S,3S,4S,6S,7R,8S,9R,10R,13S,15R)-1-benzyloxy-8-tert-butyldimethylsilyloxy-3,6;10,13-bis-epoxy-15-[N-methyl-N-(toluene-4-sulfonyl)amino]-4-phenylseleno-2,7,9-trimethyloctadecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 71098-88-9
N-phenylselanylphthalimide

: 364597-54-6
(2R,6S,7R,8R,9R,10R,13S,15R,3Z)-1-benzyloxy-8-tert-butyldimethylsilyloxy-10,13-epoxy-15-[N-methyl-N-(toluene-4-sulfonyl)amino]-2,7,9-trimethyloctadec-3-en-6-ol

: 1415891-07-4
(2S,3S,4S,6S,7R,8S,9R,10R,13S,15R)-1-benzyloxy-8-tert-butyldimethylsilyloxy-3,6;10,13-bis-epoxy-15-[N-methyl-N-(toluene-4-sulfonyl)amino]-4-phenylseleno-2,7,9-trimethyloctadecane

Guidance literature:: With zinc(II) chloride; In dichloromethane; at 20 ℃; for 2h;
DOI:10.1039/c2ob26801a

Reference yield: 85.0%

: 1415891-07-4
(2S,3S,4S,6S,7R,8S,9R,10R,13S,15R)-1-benzyloxy-8-tert-butyldimethylsilyloxy-3,6;10,13-bis-epoxy-15-[N-methyl-N-(toluene-4-sulfonyl)amino]-4-phenylseleno-2,7,9-trimethyloctadecane

: 364597-55-7
(2S,3R,6S,7R,8S,9R,10R,13S,15R)-1-benzyloxy-8-tert-butyldimethylsilyloxy-3,6;10,13-bis-epoxy-15-[N-methyl-N-(toluene-4-sulfonyl)amino]-2,7,9-trimethyloctadecane

Guidance literature:: With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In benzene; for 0.75h; Reflux;
DOI:10.1039/c2ob26801a

Reference yield:

: 1415891-07-4
(2S,3S,4S,6S,7R,8S,9R,10R,13S,15R)-1-benzyloxy-8-tert-butyldimethylsilyloxy-3,6;10,13-bis-epoxy-15-[N-methyl-N-(toluene-4-sulfonyl)amino]-4-phenylseleno-2,7,9-trimethyloctadecane

: 364597-91-1
(2S,3R,6S,7R,8S,9R,10R,13S,15R)-1-benzyloxy-8-tert-butyldimethylsilyloxy-3,6;10,13-bis-epoxy-15-(N-methylamino)-2,7,9-trimethyloctadecane

Guidance literature:: Multi-step reaction with 2 steps

1: tri-n-butyl-tin hydride; 2,2'-azobis(isobutyronitrile) / benzene / 0.75 h / Reflux

2: sodium; naphthalene / 1,2-dimethoxyethane / 1 h / -60 °C

With naphthalene; 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; sodium; In 1,2-dimethoxyethane; benzene;
DOI:10.1039/c2ob26801a