(3R,3aS,6R,6aR)-6-hydroxy-3-(4-methoxyphenyl)sulfonyloxyperhydrofuro[3,2-b]furan

Base Information

• Chemical Name: (3R,3aS,6R,6aR)-6-hydroxy-3-(4-methoxyphenyl)sulfonyloxyperhydrofuro[3,2-b]furan
• CAS No.: 72631-59-5
• Molecular Formula: C₁₃H₁₆O₆S
• Molecular Weight: 300.332

Synonyms:(3R,3aS,6R,6aR)-6-hydroxy-3-(4-methoxyphenyl)sulfonyloxyperhydrofuro[3,2-b]furan

Chemical Property of (3R,3aS,6R,6aR)-6-hydroxy-3-(4-methoxyphenyl)sulfonyloxyperhydrofuro[3,2-b]furan

Chemical Property:

Purity/Quality:

97% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (3R,3aS,6R,6aR)-6-hydroxy-3-(4-methoxyphenyl)sulfonyloxyperhydrofuro[3,2-b]furan

There total 5 articles about (3R,3aS,6R,6aR)-6-hydroxy-3-(4-methoxyphenyl)sulfonyloxyperhydrofuro[3,2-b]furan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

p-toluenesulfonyl chloride (98-59-9) + 1,4:3,6-dianhydro-D-mannitol (641-74-7) → (3R,3aS,6R,6aR)-6-hydroxy-3-(4-methoxyphenyl)sulfonyloxyperhydrofuro[3,2-b]furan (72631-59-5)

Guidance literature:

With potassium hydroxide; In water; toluene; at 4 - 5 ℃; for 4h; Industry scale;

Reference yield: 67.0%

p-toluenesulfonyl chloride (98-59-9) + 1,4:3,6-dianhydro-D-mannitol (641-74-7) → (3R,3aS,6R,6aR)-6-hydroxy-3-(4-methoxyphenyl)sulfonyloxyperhydrofuro[3,2-b]furan (72631-59-5) + (3R,3aS,6R,6aS)-hexahydrofuro[3,2-b]furan-3,6-diyl bis(4-methylbenzenesulfonate) (54522-28-0,66966-12-9,67890-26-0,76793-35-6,107740-09-0)

Guidance literature:

With pyridine; In dichloromethane;

DOI:10.1016/j.carres.2010.11.011

Reference yield: 60.0%

p-toluenesulfonyl chloride (98-59-9) + (3R,6R)-hexahydrofuro[3,2-b]furan-3,6-diol → (3R,3aS,6R,6aR)-6-hydroxy-3-(4-methoxyphenyl)sulfonyloxyperhydrofuro[3,2-b]furan (72631-59-5)

Guidance literature:

With pyridine; at 0 - 20 ℃; for 2h; Product distribution / selectivity;

upstream raw materials:

p-toluenesulfonyl chloride

1,4:3,6-dianhydro-D-mannitol

mannitol

Downstream raw materials:

(3R,3aS,6R,6aR)-6-(benzyloxy)-3-[(4-methylphenyl)sulfonyloxy]hexahydrofuro[3,2-b]furan

(3R,3aS,6R,6aR)-6-(allyloxy)-3-[(4-methylphenyl)sulfonyloxy]hexahydrofuro[3,2-b]furan

(3R,3aR,6R,6aR)-3-tert-butyldimethylsilyloxi-6-p-toluenosulfonyloxy-1,4-dioxabicyclo[3.3.0]octane

(3R,3aR,6S,6aR)-3-hydroxy-6-(3'-methylimidazolium)-1,4-dioxabicyclo[3.3.0]octane tosylate

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 72631-59-5 (3R,3aS,6R,6aR)-6-hydroxy-3-(4-methoxyphenyl)sulfonyloxyperhydrofuro[3,2-b]furan

Send

Send

Metric Ton KG G Pound L ML

Send

Send