1-(3-(trifluoromethyl)phenylsulfonyl)piperidin-4-one O-(4-fluorophenyl)(methyl)carbamoyl oxime

Base Information

Chemical Name:1-(3-(trifluoromethyl)phenylsulfonyl)piperidin-4-one O-(4-fluorophenyl)(methyl)carbamoyl oxime
CAS No.:1092464-10-2
Molecular Formula:C₂₀H₁₉F₄N₃O₄S
Molecular Weight:473.448
Hs Code.:

Synonyms:1-(3-(trifluoromethyl)phenylsulfonyl)piperidin-4-one O-(4-fluorophenyl)(methyl)carbamoyl oxime

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Chemical Property of 1-(3-(trifluoromethyl)phenylsulfonyl)piperidin-4-one O-(4-fluorophenyl)(methyl)carbamoyl oxime

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Technology Process of 1-(3-(trifluoromethyl)phenylsulfonyl)piperidin-4-one O-(4-fluorophenyl)(methyl)carbamoyl oxime

There total 2 articles about 1-(3-(trifluoromethyl)phenylsulfonyl)piperidin-4-one O-(4-fluorophenyl)(methyl)carbamoyl oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 1092464-43-1
1-(3-(trifluoromethyl)phenylsulfonyl)piperidin-4-one oxime

: 459-59-6
4-fluoro-N-methylaniline

: 503-38-8
trichloromethyl chloroformate

: 1092464-10-2
1-(3-(trifluoromethyl)phenylsulfonyl)piperidin-4-one O-(4-fluorophenyl)(methyl)carbamoyl oxime

Guidance literature:: 1-(3-(trifluoromethyl)phenylsulfonyl)piperidin-4-one oxime; trichloromethyl chloroformate; In tetrahydrofuran; at 0 - 20 ℃; for 16h;

4-fluoro-N-methylaniline; With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; at 20 ℃; for 16h;

Reference yield:

: 216983-38-9
1-(3-(trifluoromethyl)phenylsulfonyl)piperidin-4-one

: 1092464-10-2
1-(3-(trifluoromethyl)phenylsulfonyl)piperidin-4-one O-(4-fluorophenyl)(methyl)carbamoyl oxime

Guidance literature:: Multi-step reaction with 2 steps

1.1: pyridine; hydroxylamine hydrochloride / 3 h / 20 °C

2.1: tetrahydrofuran / 16 h / 0 - 20 °C

2.2: 16 h / 20 °C

With pyridine; hydroxylamine hydrochloride; In tetrahydrofuran;