3-benzo[1,3]dioxol-5-yl-4-(3-(2-{2-[2-(2-azidoethoxy)ethoxy]ethoxy}ethoxy)-4,5-dimethoxybenzyl)-5-hydroxy-5-(4-methoxyphenyl)-5H-furan-2-one

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Chemical Name:3-benzo[1,3]dioxol-5-yl-4-(3-(2-{2-[2-(2-azidoethoxy)ethoxy]ethoxy}ethoxy)-4,5-dimethoxybenzyl)-5-hydroxy-5-(4-methoxyphenyl)-5H-furan-2-one
CAS No.:928837-33-6
Molecular Formula:C₃₅H₃₉N₃O₁₂
Molecular Weight:693.708
Hs Code.:

Synonyms:3-benzo[1,3]dioxol-5-yl-4-(3-(2-{2-[2-(2-azidoethoxy)ethoxy]ethoxy}ethoxy)-4,5-dimethoxybenzyl)-5-hydroxy-5-(4-methoxyphenyl)-5H-furan-2-one

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Chemical Property of 3-benzo[1,3]dioxol-5-yl-4-(3-(2-{2-[2-(2-azidoethoxy)ethoxy]ethoxy}ethoxy)-4,5-dimethoxybenzyl)-5-hydroxy-5-(4-methoxyphenyl)-5H-furan-2-one

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Technology Process of 3-benzo[1,3]dioxol-5-yl-4-(3-(2-{2-[2-(2-azidoethoxy)ethoxy]ethoxy}ethoxy)-4,5-dimethoxybenzyl)-5-hydroxy-5-(4-methoxyphenyl)-5H-furan-2-one

There total 3 articles about 3-benzo[1,3]dioxol-5-yl-4-(3-(2-{2-[2-(2-azidoethoxy)ethoxy]ethoxy}ethoxy)-4,5-dimethoxybenzyl)-5-hydroxy-5-(4-methoxyphenyl)-5H-furan-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 928837-32-5
3-(2-{2-[2-(2-azidoethoxy)ethox]ethoxy}ethoxy)-4,5-dimethoxybenzaldehyde

: 162256-49-7
2-benzo<1,3>dioxol-5-yl-4-(4-methoxyphenyl)-4-oxobutyric acid methyl ester

: 928837-33-6
3-benzo[1,3]dioxol-5-yl-4-(3-(2-{2-[2-(2-azidoethoxy)ethoxy]ethoxy}ethoxy)-4,5-dimethoxybenzyl)-5-hydroxy-5-(4-methoxyphenyl)-5H-furan-2-one

Guidance literature:: 3-(2-{2-[2-(2-azidoethoxy)ethox]ethoxy}ethoxy)-4,5-dimethoxybenzaldehyde; 2-benzo<1,3>dioxol-5-yl-4-(4-methoxyphenyl)-4-oxobutyric acid methyl ester; With sodium methylate; In methanol; at 0 ℃; for 15h; Heating / reflux;

With acetic acid; In methanol; for 5h; Product distribution / selectivity; Heating / reflux;

Reference yield:

: 134179-43-4
11-azide-1-{(methylsulfonyl)oxy}-3,6,9-trioxaundecane

: 928837-33-6
3-benzo[1,3]dioxol-5-yl-4-(3-(2-{2-[2-(2-azidoethoxy)ethoxy]ethoxy}ethoxy)-4,5-dimethoxybenzyl)-5-hydroxy-5-(4-methoxyphenyl)-5H-furan-2-one

Guidance literature:: Multi-step reaction with 2 steps

1.1: caesium carbonate / N,N-dimethyl-formamide / 1.5 h / 90 °C

2.1: sodium / methanol / 19 h / Reflux

2.2: 7 h / Reflux

With sodium; caesium carbonate; In methanol; N,N-dimethyl-formamide;
DOI:10.1021/jm101110w

Reference yield:

: 29865-90-5
3-hydroxy-4,5-dimethoxybenzaldehyde

: 928837-33-6
3-benzo[1,3]dioxol-5-yl-4-(3-(2-{2-[2-(2-azidoethoxy)ethoxy]ethoxy}ethoxy)-4,5-dimethoxybenzyl)-5-hydroxy-5-(4-methoxyphenyl)-5H-furan-2-one

Guidance literature:: Multi-step reaction with 2 steps

1.1: caesium carbonate / N,N-dimethyl-formamide / 1.5 h / 90 °C

2.1: sodium / methanol / 19 h / Reflux

2.2: 7 h / Reflux

With sodium; caesium carbonate; In methanol; N,N-dimethyl-formamide;
DOI:10.1021/jm101110w