2-(3-phenylprop-2-ynyl)aniline

Base Information

Chemical Name:2-(3-phenylprop-2-ynyl)aniline
CAS No.:1159987-17-3
Molecular Formula:C₁₅H₁₃N
Molecular Weight:207.275
Hs Code.:

Synonyms:2-(3-phenylprop-2-ynyl)aniline

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(3-phenylprop-2-ynyl)aniline

Chemical Property:

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Technology Process of 2-(3-phenylprop-2-ynyl)aniline

There total 3 articles about 2-(3-phenylprop-2-ynyl)aniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1159987-56-0
C₂₀H₂₁NO₂

: 1159987-17-3
2-(3-phenylprop-2-ynyl)aniline

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 1h;
DOI:10.1021/ja903547q

Reference yield: 55.0%

: 1159987-75-3
C₁₅H₁₁NO₂

: 1159987-17-3
2-(3-phenylprop-2-ynyl)aniline

Guidance literature:: With sodium tetrahydroborate; tin(II) chloride dihdyrate; In methanol; at 0 ℃;
DOI:10.1021/ja903547q

Reference yield:

: 166329-43-7
N-tert-butoxycarbonyl-2-bromomethylaniline

: 1159987-17-3
2-(3-phenylprop-2-ynyl)aniline

Guidance literature:: Multi-step reaction with 2 steps

1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂ / tetrahydrofuran / 12 h / 60 °C / Inert atmosphere

2: dichloromethane; trifluoroacetic acid / 3 h / 20 °C / Inert atmosphere

With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; In tetrahydrofuran; dichloromethane; trifluoroacetic acid;
DOI:10.1021/acs.organomet.9b00183