(S)-valinol-tert-butyl ether formamidine of 7-benzyloxy-6-methoxy-1,2,3,4-tetrahydroisoquinoline

Base Information

Chemical Name:(S)-valinol-tert-butyl ether formamidine of 7-benzyloxy-6-methoxy-1,2,3,4-tetrahydroisoquinoline
CAS No.:133320-18-0
Molecular Formula:C₂₇H₃₈N₂O₃
Molecular Weight:438.61
Hs Code.:

Synonyms:(S)-valinol-tert-butyl ether formamidine of 7-benzyloxy-6-methoxy-1,2,3,4-tetrahydroisoquinoline

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Chemical Property of (S)-valinol-tert-butyl ether formamidine of 7-benzyloxy-6-methoxy-1,2,3,4-tetrahydroisoquinoline

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Technology Process of (S)-valinol-tert-butyl ether formamidine of 7-benzyloxy-6-methoxy-1,2,3,4-tetrahydroisoquinoline

There total 6 articles about (S)-valinol-tert-butyl ether formamidine of 7-benzyloxy-6-methoxy-1,2,3,4-tetrahydroisoquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 114926-73-7
(S)-N,N-dimethyl-N'-(tert-butoxy-2-amino-3-methylbuthyl)formamidine

: 148776-16-3
7-benzyloxy-6-methoxy-1,2,3,4-tetrahydroisoquinoline

: 133320-18-0
(S)-valinol-tert-butyl ether formamidine of 7-benzyloxy-6-methoxy-1,2,3,4-tetrahydroisoquinoline

Guidance literature:: With ammonium sulfate; In toluene; for 48h; Heating;

Reference yield:

: 2426-87-1
3-methoxy-4-(phenylmethoxy)benzaldehyde

: 133320-18-0
(S)-valinol-tert-butyl ether formamidine of 7-benzyloxy-6-methoxy-1,2,3,4-tetrahydroisoquinoline

Guidance literature:: Multi-step reaction with 4 steps

1: 73 percent / ammonium acetate / 1.5 h / Heating

2: 55 percent / lithium aluminum hydride / diethyl ether; tetrahydrofuran / 1.) reflux, 2 h, 2.) room temperature, overnight

3: formic acid / 48 h / 50 °C

4: 88 percent / ammonium sulfate / toluene / 48 h / Heating

With ammonium acetate; ammonium sulfate; lithium aluminium tetrahydride; In tetrahydrofuran; formic acid; diethyl ether; toluene;

Reference yield:

: 22231-61-4
2-[4-(benzyloxy)-3-methoxyphenyl]ethylamine

: 133320-18-0
(S)-valinol-tert-butyl ether formamidine of 7-benzyloxy-6-methoxy-1,2,3,4-tetrahydroisoquinoline

Guidance literature:: Multi-step reaction with 2 steps

1: formic acid / 48 h / 50 °C

2: 88 percent / ammonium sulfate / toluene / 48 h / Heating

With ammonium sulfate; In formic acid; toluene;