1'-benzyl-5'-methoxy-1',3'-dihydrospiro-[cyclopropane-1,3'-indol]-2'-one

Base Information

Chemical Name:1'-benzyl-5'-methoxy-1',3'-dihydrospiro-[cyclopropane-1,3'-indol]-2'-one
CAS No.:289906-68-9
Molecular Formula:C₁₈H₁₇NO₂
Molecular Weight:279.338
Hs Code.:

Synonyms:1'-benzyl-5'-methoxy-1',3'-dihydrospiro-[cyclopropane-1,3'-indol]-2'-one

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Chemical Property of 1'-benzyl-5'-methoxy-1',3'-dihydrospiro-[cyclopropane-1,3'-indol]-2'-one

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Technology Process of 1'-benzyl-5'-methoxy-1',3'-dihydrospiro-[cyclopropane-1,3'-indol]-2'-one

There total 6 articles about 1'-benzyl-5'-methoxy-1',3'-dihydrospiro-[cyclopropane-1,3'-indol]-2'-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 65836-82-0
1-benzyl-2,3-dihydro-5-methoxy-1H-indol-2-one

: 106-93-4
ethylene dibromide

: 289906-68-9
1'-benzyl-5'-methoxy-1',3'-dihydrospiro-[cyclopropane-1,3'-indol]-2'-one

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; at 0 ℃; for 3h;
DOI:10.1002/1522-2675(20000607)83:6<1175::AID-HLCA1175>3.0.CO;2-D

Reference yield: 72.0%

: 1-benzyl-5-methoxyspiro[indoline-3,2′-oxiran]-2-one

: 1774-47-6
trimethylsulfoxonium iodide

: 289906-68-9
1'-benzyl-5'-methoxy-1',3'-dihydrospiro-[cyclopropane-1,3'-indol]-2'-one

Guidance literature:: trimethylsulfoxonium iodide; With sodium hydride; In mineral oil; at 25 ℃; for 0.0833333h; Inert atmosphere;

1-benzyl-5-methoxyspiro[indoline-3,2′-oxiran]-2-one; In dimethyl sulfoxide; mineral oil; for 3h; Inert atmosphere;
DOI:10.1021/acs.orglett.8b01840

Reference yield: 61.0%

: 1774-47-6
trimethylsulfoxonium iodide

: 16077-10-4
N-benzyl-5-methoxyisatin

: 289906-68-9
1'-benzyl-5'-methoxy-1',3'-dihydrospiro-[cyclopropane-1,3'-indol]-2'-one

Guidance literature:: trimethylsulfoxonium iodide; With sodium hydride; In dimethyl sulfoxide; at 25 ℃; for 0.0833333h; Inert atmosphere;

N-benzyl-5-methoxyisatin; In dimethyl sulfoxide; for 3h; Inert atmosphere;
DOI:10.1021/acs.orglett.8b01840