ethyl 3-O-benzyl-4,6-O-benzylidene-2-O-fluorenylmethoxycarbonyl-1-thio-β-D-glucopyranoside

Base Information

Chemical Name:ethyl 3-O-benzyl-4,6-O-benzylidene-2-O-fluorenylmethoxycarbonyl-1-thio-β-D-glucopyranoside
CAS No.:1011736-84-7
Molecular Formula:C₃₇H₃₆O₇S
Molecular Weight:624.755
Hs Code.:

Synonyms:ethyl 3-O-benzyl-4,6-O-benzylidene-2-O-fluorenylmethoxycarbonyl-1-thio-β-D-glucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ethyl 3-O-benzyl-4,6-O-benzylidene-2-O-fluorenylmethoxycarbonyl-1-thio-β-D-glucopyranoside

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Technology Process of ethyl 3-O-benzyl-4,6-O-benzylidene-2-O-fluorenylmethoxycarbonyl-1-thio-β-D-glucopyranoside

There total 1 articles about ethyl 3-O-benzyl-4,6-O-benzylidene-2-O-fluorenylmethoxycarbonyl-1-thio-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 28920-43-6
(fluorenylmethoxy)carbonyl chloride

: 141810-60-8
ethyl 3-O-benzyl-4,6-O-benzylidene-1-thio-β-D-glucopyranoside

: 1011736-84-7
ethyl 3-O-benzyl-4,6-O-benzylidene-2-O-fluorenylmethoxycarbonyl-1-thio-β-D-glucopyranoside

Guidance literature:: With pyridine; at 20 ℃; for 2.5h;
DOI:10.1021/ol7030262

Reference yield: 89.0%

: 1011736-84-7
ethyl 3-O-benzyl-4,6-O-benzylidene-2-O-fluorenylmethoxycarbonyl-1-thio-β-D-glucopyranoside

: 1163704-48-0
ethyl 3,4-di-O-benzyl-2-O-(9-fluorenyl)methoxycarbonyl-1-thio-β-D-glucopyranoside

Guidance literature:: With borane-THF; trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at 20 ℃; regioselective reaction; Inert atmosphere;
DOI:10.1016/j.tetlet.2009.03.194

Reference yield: 82.0%

: 1011736-82-5
C₂₅H₃₂Cl₃NO₈

: 1011736-84-7
ethyl 3-O-benzyl-4,6-O-benzylidene-2-O-fluorenylmethoxycarbonyl-1-thio-β-D-glucopyranoside

: 1011736-88-1
C₆₀H₆₂Cl₃NO₁₅

Guidance literature:: With methyl trifluoromethanesulfonate; 2,4,6-tri-tert-butylpyrimidine; In dichloromethane; at 0 - 20 ℃; Molecular sieve;
DOI:10.1021/ol7030262