N-ethyl-N-propylammonium methyl (6-chloro-5-methoxy-2-methyl-1H-indol-3-yl)acetate

Base Information

Chemical Name:N-ethyl-N-propylammonium methyl (6-chloro-5-methoxy-2-methyl-1H-indol-3-yl)acetate
CAS No.:926624-33-1
Molecular Formula:C₅H₁₃N*C₁₂H₁₂ClNO₃
Molecular Weight:340.85
Hs Code.:

Synonyms:N-ethyl-N-propylammonium methyl (6-chloro-5-methoxy-2-methyl-1H-indol-3-yl)acetate

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Chemical Property of N-ethyl-N-propylammonium methyl (6-chloro-5-methoxy-2-methyl-1H-indol-3-yl)acetate

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Technology Process of N-ethyl-N-propylammonium methyl (6-chloro-5-methoxy-2-methyl-1H-indol-3-yl)acetate

There total 1 articles about N-ethyl-N-propylammonium methyl (6-chloro-5-methoxy-2-methyl-1H-indol-3-yl)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 123-76-2
levulinic acid

: 54812-55-4
(3-chloro-4-methoxyphenyl)hydrazine hydrochloride

: 1049806-14-5
2-(3-chloro-4-methoxyphenyl)-6-methyl-4,5-dihydropyridazin-3(2H)-one

: N-ethyl-N-propylammonium (4-chloro-5-methoxy-2-methyl-1H-indol-3-yl)acetate

: 926624-33-1
N-ethyl-N-propylammonium methyl (6-chloro-5-methoxy-2-methyl-1H-indol-3-yl)acetate

Guidance literature:: In acetic acid; at 100 ℃; for 2h;

Reference yield:

: 926624-33-1
N-ethyl-N-propylammonium methyl (6-chloro-5-methoxy-2-methyl-1H-indol-3-yl)acetate

: (6-chloro-5-methoxy-2-methyl-1-(3-trifluoromethoxybenzyl)-1H-indol-3-yl)acetic acid, lithium salt

Guidance literature:: Multi-step reaction with 3 steps

1.1: sulfuric acid / 2 h / 30 °C

2.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 5 °C

2.2: 2.5 h / 12 °C

3.1: lithium hydroxide; water / tetrahydrofuran; methanol / 3 h

With lithium hydroxide; sulfuric acid; water; sodium hydride; In tetrahydrofuran; methanol; N,N-dimethyl-formamide;

Reference yield:

: 926624-33-1
N-ethyl-N-propylammonium methyl (6-chloro-5-methoxy-2-methyl-1H-indol-3-yl)acetate

: {6-chloro-5-methoxy-2-methyl-1-[3-(trifluoromethoxy)benzyl]-1H-indol-3-yl}acetic acid

Guidance literature:: Multi-step reaction with 4 steps

1.1: sulfuric acid / 2 h / 30 °C

2.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 5 °C

2.2: 2.5 h / 12 °C

3.1: lithium hydroxide; water / tetrahydrofuran; methanol / 3 h

4.1: hydrogenchloride / water; ethyl acetate

With hydrogenchloride; lithium hydroxide; sulfuric acid; water; sodium hydride; In tetrahydrofuran; methanol; water; ethyl acetate; N,N-dimethyl-formamide;