1-benzyl 2-methyl (2S,3aR,8aS)-6-chloro-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-3a-((triethylsilyl)oxy)-3,3a,8,8a-tetrahydropyrrolo[2,3-b]indole-1,2(2H)-dicarboxylate

Base Information

Chemical Name:1-benzyl 2-methyl (2S,3aR,8aS)-6-chloro-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-3a-((triethylsilyl)oxy)-3,3a,8,8a-tetrahydropyrrolo[2,3-b]indole-1,2(2H)-dicarboxylate
CAS No.:1301725-50-7
Molecular Formula:C₃₂H₄₄BClN₂O₇Si
Molecular Weight:643.06
Hs Code.:

1-benzyl 2-methyl (2S,3aR,8aS)-6-chloro-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-3a-((triethylsilyl)oxy)-3,3a,8,8a-tetrahydropyrrolo[2,3-b]indole-1,2(2H)-dicarboxylate

Synonyms:1-benzyl 2-methyl (2S,3aR,8aS)-6-chloro-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-3a-((triethylsilyl)oxy)-3,3a,8,8a-tetrahydropyrrolo[2,3-b]indole-1,2(2H)-dicarboxylate

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Chemical Property of 1-benzyl 2-methyl (2S,3aR,8aS)-6-chloro-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-3a-((triethylsilyl)oxy)-3,3a,8,8a-tetrahydropyrrolo[2,3-b]indole-1,2(2H)-dicarboxylate

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Technology Process of 1-benzyl 2-methyl (2S,3aR,8aS)-6-chloro-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-3a-((triethylsilyl)oxy)-3,3a,8,8a-tetrahydropyrrolo[2,3-b]indole-1,2(2H)-dicarboxylate

There total 2 articles about 1-benzyl 2-methyl (2S,3aR,8aS)-6-chloro-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-3a-((triethylsilyl)oxy)-3,3a,8,8a-tetrahydropyrrolo[2,3-b]indole-1,2(2H)-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 1248759-39-8
1-benzyl 2-methyl (2S,3aR,8aS)-6-chloro-5-iodo-3a-((triethylsilyl)oxy)-3,3a,8,8a-tetrahydropyrrolo[2,3-b]indole-1,2(2H)-dicarboxylate

: 73183-34-3
bis(pinacol)diborane

: 1301725-50-7
1-benzyl 2-methyl (2S,3aR,8aS)-6-chloro-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-3a-((triethylsilyl)oxy)-3,3a,8,8a-tetrahydropyrrolo[2,3-b]indole-1,2(2H)-dicarboxylate

Guidance literature:: With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate; In dimethyl sulfoxide; at 80 ℃; for 0.75h;
DOI:10.1002/chem.201003216

Reference yield: 37.0%

: 1248759-39-8
1-benzyl 2-methyl (2S,3aR,8aS)-6-chloro-5-iodo-3a-((triethylsilyl)oxy)-3,3a,8,8a-tetrahydropyrrolo[2,3-b]indole-1,2(2H)-dicarboxylate

: 73183-34-3
bis(pinacol)diborane

: 1301725-52-9
C₂₆H₃₀BClN₂O₇

: 1301725-50-7
1-benzyl 2-methyl (2S,3aR,8aS)-6-chloro-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-3a-((triethylsilyl)oxy)-3,3a,8,8a-tetrahydropyrrolo[2,3-b]indole-1,2(2H)-dicarboxylate

Guidance literature:: With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate; In dimethyl sulfoxide; at 80 ℃;
DOI:10.1002/chem.201003216

Reference yield: 36.0%

: 1248759-39-8
1-benzyl 2-methyl (2S,3aR,8aS)-6-chloro-5-iodo-3a-((triethylsilyl)oxy)-3,3a,8,8a-tetrahydropyrrolo[2,3-b]indole-1,2(2H)-dicarboxylate

: 1301725-50-7
1-benzyl 2-methyl (2S,3aR,8aS)-6-chloro-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-3a-((triethylsilyl)oxy)-3,3a,8,8a-tetrahydropyrrolo[2,3-b]indole-1,2(2H)-dicarboxylate

: 1248759-45-6
1,1'-dibenzyl 2,2'-dimethyl (2S,2'S,3aR,3a'R,8aS,8a'S)-6,6'-dichloro-3a,3a'-bis((triethylsilyl)oxy)-3,3',3a,3a',8,8',8a,8a'-octahydro-5,5'-bipyrrolo[2,3-b]indole-1,1',2,2'(2H,2'H)-tetracarboxylate

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium hydroxide; In water; toluene; at 50 ℃;
DOI:10.1002/chem.201003216