2''-O-acetyl-4'',6''-O-benzylidene-1,3,2',6',3''-penta-N-tosyldibekacin

Base Information

Chemical Name:2''-O-acetyl-4'',6''-O-benzylidene-1,3,2',6',3''-penta-N-tosyldibekacin
CAS No.:190430-66-1
Molecular Formula:C₆₂H₇₃N₅O₁₉S₅
Molecular Weight:1352.61
Hs Code.:

Synonyms:2''-O-acetyl-4'',6''-O-benzylidene-1,3,2',6',3''-penta-N-tosyldibekacin

Suppliers and Price of 2''-O-acetyl-4'',6''-O-benzylidene-1,3,2',6',3''-penta-N-tosyldibekacin

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2''-O-acetyl-4'',6''-O-benzylidene-1,3,2',6',3''-penta-N-tosyldibekacin

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Technology Process of 2''-O-acetyl-4'',6''-O-benzylidene-1,3,2',6',3''-penta-N-tosyldibekacin

There total 3 articles about 2''-O-acetyl-4'',6''-O-benzylidene-1,3,2',6',3''-penta-N-tosyldibekacin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 75-36-5
acetyl chloride

: 4'',6''-O-benzylidene-1,3,2',6',3''-penta-N-tosyldibekacin

: 190430-66-1
2''-O-acetyl-4'',6''-O-benzylidene-1,3,2',6',3''-penta-N-tosyldibekacin

Guidance literature:: In pyridine; for 3h; Ambient temperature;
DOI:10.1016/S0008-6215(97)00031-1

Reference yield:

: 64879-65-8
3',4'-dideoxy-5-fluoro-1,3,2',6',3''-penta-N-tosylkanamycin B

: 190430-66-1
2''-O-acetyl-4'',6''-O-benzylidene-1,3,2',6',3''-penta-N-tosyldibekacin

Guidance literature:: Multi-step reaction with 2 steps

1: TsOH / dimethylformamide / 50 °C

2: 84 percent / pyridine / 3 h / Ambient temperature

With toluene-4-sulfonic acid; In pyridine; N,N-dimethyl-formamide;
DOI:10.1016/S0008-6215(97)00031-1

Reference yield:

: 1125-88-8
benzaldehyde dimethyl acetal

: 190430-66-1
2''-O-acetyl-4'',6''-O-benzylidene-1,3,2',6',3''-penta-N-tosyldibekacin

Guidance literature:: Multi-step reaction with 2 steps

1: TsOH / dimethylformamide / 50 °C

2: 84 percent / pyridine / 3 h / Ambient temperature

With toluene-4-sulfonic acid; In pyridine; N,N-dimethyl-formamide;
DOI:10.1016/S0008-6215(97)00031-1