trimethylsilane adduct of trimethylsilylium tetrakis(pentafluorophenyl)borate

Base Information

• Chemical Name: trimethylsilane adduct of trimethylsilylium tetrakis(pentafluorophenyl)borate
• CAS No.: 1331770-02-5
• Molecular Formula: C₆H₁₉Si₂*C₂₄BF₂₀
• Molecular Weight: 826.431
• Mol file: 1331770-02-5.mol

Synonyms:trimethylsilane adduct of trimethylsilylium tetrakis(pentafluorophenyl)borate

Chemical Property of trimethylsilane adduct of trimethylsilylium tetrakis(pentafluorophenyl)borate

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of trimethylsilane adduct of trimethylsilylium tetrakis(pentafluorophenyl)borate

There total 1 articles about trimethylsilane adduct of trimethylsilylium tetrakis(pentafluorophenyl)borate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

trimethylsilan (993-07-7) + trityl tetrakis(pentafluorophenyl)borate → trimethylsilane adduct of trimethylsilylium tetrakis(pentafluorophenyl)borate (1331770-02-5)

Guidance literature:

at 20 ℃; for 12h; Inert atmosphere; Schlenk technique;

DOI:10.1021/om500519j

Reference yield: 83.0%

Tris(trimethylsilyl) phosphate (10497-05-9) + trimethylsilane adduct of trimethylsilylium tetrakis(pentafluorophenyl)borate (1331770-02-5) → tetrakis(trimethylsiloxy)phosphonium tetrakis(pentafluorophenyl)borate

Guidance literature:

In toluene; for 1h; Sonication;

DOI:10.1021/acs.inorgchem.8b01323

Reference yield: 77.0%

bis(trimethylsilyl)carbodi-imide (1000-70-0) + trimethylsilane adduct of trimethylsilylium tetrakis(pentafluorophenyl)borate (1331770-02-5) → N,N-bis(trimethylsilyl)amino-N-(trimethylsilyl)nitrilium tetrakis(pentafluorophenyl)borate (1402147-89-0)

Guidance literature:

In toluene; at 20 ℃; Inert atmosphere;

DOI:10.1021/ja308104k

upstream raw materials:

trimethylsilan

Downstream raw materials:

4,5,6,7-tetrafluorobenzo[1,3]dithiol-2-ylidene tris(pentafluorophenyl)borane

tris(pentafluorophenyl)borate

1,4-di-tert-butylbenzene

bis(trimethylsilyl)fluoronium tetrakis(pentafluorophenyl)borate