O-pinacolyl p-nitrophenyl methylphosphonate

Base Information

Chemical Name:O-pinacolyl p-nitrophenyl methylphosphonate
CAS No.:349609-58-1
Molecular Formula:C₁₃H₂₀NO₅P
Molecular Weight:301.279
Hs Code.:

Synonyms:O-pinacolyl p-nitrophenyl methylphosphonate

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Chemical Property of O-pinacolyl p-nitrophenyl methylphosphonate

Chemical Property:

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Technology Process of O-pinacolyl p-nitrophenyl methylphosphonate

There total 7 articles about O-pinacolyl p-nitrophenyl methylphosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: O-pinacolyl p-nitrophenyl methylphosphonate

: 349609-58-1
O-pinacolyl p-nitrophenyl methylphosphonate

Guidance literature:: With CHES buffer; phosphotriesterase G₆₀A mutant enzyme; In water; acetonitrile; at 20 ℃; pH=9.0;
DOI:10.1016/S0968-0896(01)00113-4

Reference yield:

: 676-97-1
methylphosphonic acid dichloroanhydride

: 100-02-7,78813-13-5,89830-32-0
4-nitro-phenol

: 1517-67-5
(S)-3,3-dimethylbutan-2-ol

: 349609-58-1
O-pinacolyl p-nitrophenyl methylphosphonate

: 349609-57-0
R_P-O-(S_C)-pinacolyl p-nitrophenyl methylphosphonate

Guidance literature:: (S)-3,3-dimethylbutan-2-ol; With lithium diisopropyl amide; In tetrahydrofuran; diethyl ether; at -78 ℃; for 0.5h;

methylphosphonic acid dichloroanhydride; In diethyl ether; at -78 - 23 ℃; for 6h;

4-nitro-phenol; With triethylamine; at 23 ℃; for 16h;
DOI:10.1021/acs.biochem.1c00361

Reference yield:

: O-pinacolyl p-nitrophenyl methylphosphonate

: 349609-58-1
O-pinacolyl p-nitrophenyl methylphosphonate

: 349609-57-0
R_P-O-(S_C)-pinacolyl p-nitrophenyl methylphosphonate

Guidance literature:: With CHES buffer; H₂₅₇Y mutant enzyme; phosphotriesterase I₁₀₆A; In water; acetonitrile; at 20 ℃; pH=9.0; Title compound not separated from byproducts;
DOI:10.1016/S0968-0896(01)00113-4