Technology Process of C28H32N2O9S
There total 3 articles about C28H32N2O9S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C25H28N2O7S; chloroformic acid ethyl ester;
With
triethylamine;
In
dichloromethane;
at 20 ℃;
for 3h;
With
sodium cyanoborohydride;
In
methanol;
at 20 ℃;
for 1h;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: potassium carbonate / N,N-dimethyl-formamide / 3 h / 20 °C
2: borane-THF / tetrahydrofuran / 5 h / Reflux
3: triethylamine / methanol / 20 °C
4: hydrogen; palladium on activated charcoal / methanol / 8 h / 20 °C
5: triethylamine / dichloromethane / 3 h / 20 °C
With
borane-THF; palladium on activated charcoal; hydrogen; potassium carbonate; triethylamine;
In
tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: borane-THF / tetrahydrofuran / 5 h / Reflux
2: triethylamine / methanol / 20 °C
3: hydrogen; palladium on activated charcoal / methanol / 8 h / 20 °C
4: triethylamine / dichloromethane / 3 h / 20 °C
With
borane-THF; palladium on activated charcoal; hydrogen; triethylamine;
In
tetrahydrofuran; methanol; dichloromethane;