[2R-(2α,3α,4β,5α,6β)]-3,4,5-tris (phenylmethoxy)-6-[(phenylmethoxy)methyl]-1-(phenylmethyl)-2-piperidinemethanol

Base Information

Chemical Name:[2R-(2α,3α,4β,5α,6β)]-3,4,5-tris (phenylmethoxy)-6-[(phenylmethoxy)methyl]-1-(phenylmethyl)-2-piperidinemethanol
CAS No.:137326-11-5
Molecular Formula:C₄₂H₄₅NO₅
Molecular Weight:643.823
Hs Code.:

Synonyms:[2R-(2α,3α,4β,5α,6β)]-3,4,5-tris (phenylmethoxy)-6-[(phenylmethoxy)methyl]-1-(phenylmethyl)-2-piperidinemethanol

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Chemical Property of [2R-(2α,3α,4β,5α,6β)]-3,4,5-tris (phenylmethoxy)-6-[(phenylmethoxy)methyl]-1-(phenylmethyl)-2-piperidinemethanol

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Technology Process of [2R-(2α,3α,4β,5α,6β)]-3,4,5-tris (phenylmethoxy)-6-[(phenylmethoxy)methyl]-1-(phenylmethyl)-2-piperidinemethanol

There total 6 articles about [2R-(2α,3α,4β,5α,6β)]-3,4,5-tris (phenylmethoxy)-6-[(phenylmethoxy)methyl]-1-(phenylmethyl)-2-piperidinemethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 104343-31-9
2,6-dideoxy-2,6-<<(phenylmethoxy)carbonyl>imino>-1,3,4,5-tetrakis-O-(phenylmethyl)-D-glycero-L-gulo-heptitol

: 137326-11-5
[2R-(2α,3α,4β,5α,6β)]-3,4,5-tris (phenylmethoxy)-6-[(phenylmethoxy)methyl]-1-(phenylmethyl)-2-piperidinemethanol

Guidance literature:: Multi-step reaction with 3 steps

1: 83 percent / cyclohexene / Pd/C / methanol

2: Et₃N

3: AlH₃ / tetrahydrofuran

With aluminium hydride; triethylamine; cyclohexene; palladium on activated charcoal; In tetrahydrofuran; methanol;
DOI:10.1016/S0040-4039(00)79409-3

Reference yield:

: Phenyl-((2R,3R,4R,5S,6R)-3,4,5-tris-benzyloxy-2-benzyloxymethyl-6-hydroxymethyl-piperidin-1-yl)-methanone

: 137326-11-5
[2R-(2α,3α,4β,5α,6β)]-3,4,5-tris (phenylmethoxy)-6-[(phenylmethoxy)methyl]-1-(phenylmethyl)-2-piperidinemethanol

Guidance literature:: With aluminium hydride; In tetrahydrofuran; Yield given;
DOI:10.1016/S0040-4039(00)79409-3

Reference yield:

: 110205-71-5
2,6-dideoxy-2,6-imino-1,3,4,5-tetrakis-O-(phenylmethyl)-D-glycero-L-gulo-heptitol

: 137326-11-5
[2R-(2α,3α,4β,5α,6β)]-3,4,5-tris (phenylmethoxy)-6-[(phenylmethoxy)methyl]-1-(phenylmethyl)-2-piperidinemethanol

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N

2: AlH₃ / tetrahydrofuran

With aluminium hydride; triethylamine; In tetrahydrofuran;
DOI:10.1016/S0040-4039(00)79409-3