5-(5,5-Dimethyl-1,3,2-dioxaborinan-2-yl)-1-methyl-1H-indole, 5,5-Dimethyl-2-(1-methyl-1H-indol-5-yl)-1,3,2-dioxaborinane

Base Information

Chemical Name:5-(5,5-Dimethyl-1,3,2-dioxaborinan-2-yl)-1-methyl-1H-indole, 5,5-Dimethyl-2-(1-methyl-1H-indol-5-yl)-1,3,2-dioxaborinane
CAS No.:916518-57-5
Molecular Formula:C₁₄H₁₈BNO₂
Molecular Weight:243.113
Hs Code.:2933299090
Mol file:916518-57-5.mol

Synonyms:5-(5,5-dimethyl-1,3,2-dioxaborinan-2-yl)-1-methyl-1H-indole

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Chemical Property of 5-(5,5-Dimethyl-1,3,2-dioxaborinan-2-yl)-1-methyl-1H-indole, 5,5-Dimethyl-2-(1-methyl-1H-indol-5-yl)-1,3,2-dioxaborinane

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Technology Process of 5-(5,5-Dimethyl-1,3,2-dioxaborinan-2-yl)-1-methyl-1H-indole, 5,5-Dimethyl-2-(1-methyl-1H-indol-5-yl)-1,3,2-dioxaborinane

There total 5 articles about 5-(5,5-Dimethyl-1,3,2-dioxaborinan-2-yl)-1-methyl-1H-indole, 5,5-Dimethyl-2-(1-methyl-1H-indol-5-yl)-1,3,2-dioxaborinane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 126-30-7
2,2-Dimethyl-1,3-propanediol

: 192182-55-1
(1-methyl-1H-indol-5-yl)boronic acid

: 916518-57-5
5-(5,5-dimethyl-1,3,2-dioxaborinan-2-yl)-1-methyl-1H-indole

Guidance literature:: In dichloromethane; at 20 ℃; for 12h;
DOI:10.1021/acs.orglett.9b02236

Reference yield: 53.0%

: 1268936-45-3
C₁₂H₁₄N₂O₂

: 201733-56-4
2-(5,5-dimethyl-1,3,2-dioxaborinan-2-yl)-5,5-dimethyl-1,3,2-dioxaborinane

: 916518-57-5
5-(5,5-dimethyl-1,3,2-dioxaborinan-2-yl)-1-methyl-1H-indole

Guidance literature:: With potassium phosphate; bis(tricyclohexylphosphine)nickel(II) dichloride; In 1,2-dimethoxyethane; toluene; at 120 ℃; for 48h; Inert atmosphere;
DOI:10.1002/chem.201001943

Reference yield: 47.0%

: 116176-92-2
5-fluoro-1-methyl-1H-indole

: 201733-56-4
2-(5,5-dimethyl-1,3,2-dioxaborinan-2-yl)-5,5-dimethyl-1,3,2-dioxaborinane

: 916518-57-5
5-(5,5-dimethyl-1,3,2-dioxaborinan-2-yl)-1-methyl-1H-indole

Guidance literature:: With bis(1,5-cyclooctadiene)nickel⁽⁰⁾; sodium phenoxide; tricyclohexylphosphine; In tetrahydrofuran; at 110 ℃; for 15h; Schlenk technique; Inert atmosphere; Glovebox;
DOI:10.1021/jacs.5b08103