Te-phenyl telluroacetate

Base Information

• Chemical Name: Te-phenyl telluroacetate
• CAS No.: 28231-37-0
• Molecular Formula: C₈H₈OTe
• Molecular Weight: 247.751
• Mol file: 28231-37-0.mol

Synonyms:Te-phenyl telluroacetate

Chemical Property of Te-phenyl telluroacetate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Te-phenyl telluroacetate

There total 3 articles about Te-phenyl telluroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

diphenyl ditelluride (32294-60-3) + acetic anhydride (108-24-7) → Te-phenyl telluroacetate (28231-37-0)

Guidance literature:

diphenyl ditelluride; With samarium; zirconium(IV) chloride; In tetrahydrofuran; at 20 ℃; for 2h;

acetic anhydride; In tetrahydrofuran; at 20 ℃; for 1h;

DOI:10.1080/00304949909355738

Reference yield: 59.0%

acetyl chloride (75-36-5) + phenyl tris(trimethylsilyl)silyl telluride (197724-17-7) → Te-phenyl telluroacetate (28231-37-0)

Guidance literature:

tetrakis(triphenylphosphine) palladium⁽⁰⁾; In benzene; at 25 ℃; for 2h;

DOI:10.1039/a704402j

Reference yield:

cyclohexyl phenyl telluride (56950-05-1) → Te-phenyl telluroacetate (28231-37-0)

Guidance literature:

Multi-step reaction with 2 steps

1: AIBN / benzene / 2 h / 80 °C

2: 59 percent / (Ph₃P)4Pd / benzene / 2 h / 25 °C

With 2,2'-azobis(isobutyronitrile); tetrakis(triphenylphosphine) palladium⁽⁰⁾; In benzene;

DOI:10.1039/a704402j

upstream raw materials:

diphenyl ditelluride

acetic anhydride

acetyl chloride

phenyl tris(trimethylsilyl)silyl telluride