Trisilane, 1,1,1,3,3,3-hexamethyl-2-(phenyltelluro)-2-(trimethylsilyl)-

Base Information

• Chemical Name: Trisilane, 1,1,1,3,3,3-hexamethyl-2-(phenyltelluro)-2-(trimethylsilyl)-
• CAS No.: 197724-17-7
• Molecular Formula: C15H32Si4Te
• Molecular Weight: 452.361
• DSSTox Substance ID: DTXSID70442938
• Nikkaji Number: J886.871I
• Wikidata: Q82260556
• Mol file: 197724-17-7.mol

Synonyms:Trisilane, 1,1,1,3,3,3-hexamethyl-2-(phenyltelluro)-2-(trimethylsilyl)-;197724-17-7;(Phenyltelluro)tris(trimethylsilyl)silane;DTXSID70442938

Chemical Property of Trisilane, 1,1,1,3,3,3-hexamethyl-2-(phenyltelluro)-2-(trimethylsilyl)-

Chemical Property:

• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 0
• Rotatable Bond Count: 5
• Exact Mass: 454.0643299
• Heavy Atom Count: 20
• Complexity: 280

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C[Si](C)(C)[Si]([Si](C)(C)C)([Si](C)(C)C)[Te]C1=CC=CC=C1

Technology Process of Trisilane, 1,1,1,3,3,3-hexamethyl-2-(phenyltelluro)-2-(trimethylsilyl)-

There total 1 articles about Trisilane, 1,1,1,3,3,3-hexamethyl-2-(phenyltelluro)-2-(trimethylsilyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

tris-(trimethylsilyl)silane (1873-77-4) + cyclohexyl phenyl telluride (56950-05-1) → phenyl tris(trimethylsilyl)silyl telluride (197724-17-7)

Guidance literature:

With 2,2'-azobis(isobutyronitrile); In benzene; at 80 ℃; for 2h;

DOI:10.1039/a704402j

Reference yield: 79.0%

methyl chloroformate (79-22-1) + phenyl tris(trimethylsilyl)silyl telluride (197724-17-7) → methyl (phenyltelluro)formate

Guidance literature:

tetrakis(triphenylphosphine) palladium⁽⁰⁾; In benzene; at 25 ℃; for 2h;

DOI:10.1039/a704402j

Reference yield: 72.0%

phenyl tris(trimethylsilyl)silyl telluride (197724-17-7) + cyclohexyl chloroformate (13248-54-9) → cyclohexyl (phenyltelluro)formate (180588-36-7)

Guidance literature:

tetrakis(triphenylphosphine) palladium⁽⁰⁾; In benzene; at 25 ℃; for 16h;

DOI:10.1039/a704402j

upstream raw materials:

tris-(trimethylsilyl)silane

cyclohexyl phenyl telluride

Downstream raw materials:

Te-phenyl telluroacetate

2-methyl-1-propyl (phenyltelluro)formate

cyclohexyl (phenyltelluro)formate

benzyl phenyl telluride