[(1-bis(p-fluorophenyl)phosphanyl-2-t-butylsulfenylferrocene)PdCl(CH₃)]

Base Information

Chemical Name:[(1-bis(p-fluorophenyl)phosphanyl-2-t-butylsulfenylferrocene)PdCl(CH₃)]
CAS No.:769154-28-1
Molecular Formula:C₂₇H₂₈ClF₂FePPdS
Molecular Weight:651.276
Hs Code.:

[(1-bis(p-fluorophenyl)phosphanyl-2-t-butylsulfenylferrocene)PdCl(CH<sub>3</sub>)]

Synonyms:[(1-bis(p-fluorophenyl)phosphanyl-2-t-butylsulfenylferrocene)PdCl(CH₃)]

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Chemical Property of [(1-bis(p-fluorophenyl)phosphanyl-2-t-butylsulfenylferrocene)PdCl(CH₃)]

Chemical Property:

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Technology Process of [(1-bis(p-fluorophenyl)phosphanyl-2-t-butylsulfenylferrocene)PdCl(CH₃)]

There total 2 articles about [(1-bis(p-fluorophenyl)phosphanyl-2-t-butylsulfenylferrocene)PdCl(CH₃)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 769154-22-5
[(1-bis(p-fluorophenyl)phosphanyl-2-t-butylsulfenylferrocene)PdCl₂]

: 544-97-8
dimethyl zinc(II)

: 769154-28-1
[(1-bis(p-fluorophenyl)phosphanyl-2-t-butylsulfenylferrocene)PdCl(CH₃)]

Guidance literature:: In dichloromethane; at room temp.;
DOI:10.1002/anie.200460087

Reference yield: 95.0%

: 769154-22-5
((C₅H₅)Fe(C₅H₃(SC(CH₃)3)P(C₆H₄F)2))PdCl₂

: 544-97-8
dimethyl zinc(II)

: 769154-28-1
((C₅H₅)Fe(C₅H₃(SC(CH₃)3)P(C₆H₄F)2))PdCl(CH₃)

Guidance literature:: In dichloromethane; Fe-Pd complex reacted with Me2Zn (1.5 equiv.) in CH2Cl2 at room temp.; purified by standard silica gel chromy.; detd. by (1)H and (13)C NMR spectra;
DOI:10.1021/ja055692b

Reference yield:

: 769154-28-1
((C₅H₅)Fe(C₅H₃(SC(CH₃)3)P(C₆H₄F)2))PdCl(CH₃)

: 79060-88-1
sodium tetrakis[(3,5-di-trifluoromethyl)phenyl]borate

: ((C₅H₅)Fe(C₅H₃(SC(CH₃)3)P(C₆H₄F)2))Pd(CH₃)⁽¹⁺⁾

Guidance literature:: In 1,2-dichloro-ethane; in situ; Fe-Pd complex reacted with B compd. (molar ratio 1:1) in dichloroethane; not isolated;
DOI:10.1021/ja055692b