2-chloro-N-(2-chloro-3-fluoro-pyridin-4-yl)-6-fluorobenzimidoyl chloride

Base Information

Chemical Name:2-chloro-N-(2-chloro-3-fluoro-pyridin-4-yl)-6-fluorobenzimidoyl chloride
CAS No.:1365991-98-5
Molecular Formula:C₁₂H₅Cl₃F₂N₂
Molecular Weight:321.541
Hs Code.:

Synonyms:2-chloro-N-(2-chloro-3-fluoro-pyridin-4-yl)-6-fluorobenzimidoyl chloride

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Chemical Property of 2-chloro-N-(2-chloro-3-fluoro-pyridin-4-yl)-6-fluorobenzimidoyl chloride

Chemical Property:

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Technology Process of 2-chloro-N-(2-chloro-3-fluoro-pyridin-4-yl)-6-fluorobenzimidoyl chloride

There total 5 articles about 2-chloro-N-(2-chloro-3-fluoro-pyridin-4-yl)-6-fluorobenzimidoyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1365991-97-4
2-chloro-N-(2-chloro-3-fluoro-pyridine-4-yl)-6-fluorobenzamide

: 1365991-98-5
2-chloro-N-(2-chloro-3-fluoro-pyridin-4-yl)-6-fluorobenzimidoyl chloride

Guidance literature:: With thionyl chloride; for 16h; Reflux;

Reference yield:

: 79455-63-3
2-chloro-6-fluorobenzoyl chloride

: 1365991-98-5
2-chloro-N-(2-chloro-3-fluoro-pyridin-4-yl)-6-fluorobenzimidoyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / 1,4-dioxane / 6 h / 50 °C / Reflux

2: thionyl chloride / 16 h / Reflux

With thionyl chloride; triethylamine; In 1,4-dioxane;

Reference yield:

: 628691-93-0
2-chloro-3-fluoro-pyridine-4-carboxylic acid

: 1365991-98-5
2-chloro-N-(2-chloro-3-fluoro-pyridin-4-yl)-6-fluorobenzimidoyl chloride

Guidance literature:: Multi-step reaction with 4 steps

1.1: diphenyl phosphoryl azide / toluene / 3 h / 110 °C / Inert atmosphere

2.1: trifluoroacetic acid / dichloromethane / 5 h / 20 °C

2.2: NH₂ cartridge

3.1: triethylamine / 1,4-dioxane / 6 h / 50 °C / Reflux

4.1: thionyl chloride / 16 h / Reflux

With thionyl chloride; diphenyl phosphoryl azide; triethylamine; trifluoroacetic acid; In 1,4-dioxane; dichloromethane; toluene;