[2-Butyl-5-(2-chloro-benzyl)-4,5,6,7-tetrahydro-thieno[3,2-c]pyridin-3-yl]-(4-methoxy-phenyl)-methanone

Base Information

Chemical Name:[2-Butyl-5-(2-chloro-benzyl)-4,5,6,7-tetrahydro-thieno[3,2-c]pyridin-3-yl]-(4-methoxy-phenyl)-methanone
CAS No.:749805-59-2
Molecular Formula:C₂₆H₂₈ClNO₂S
Molecular Weight:454.033
Hs Code.:

Synonyms:[2-Butyl-5-(2-chloro-benzyl)-4,5,6,7-tetrahydro-thieno[3,2-c]pyridin-3-yl]-(4-methoxy-phenyl)-methanone

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Chemical Property of [2-Butyl-5-(2-chloro-benzyl)-4,5,6,7-tetrahydro-thieno[3,2-c]pyridin-3-yl]-(4-methoxy-phenyl)-methanone

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Technology Process of [2-Butyl-5-(2-chloro-benzyl)-4,5,6,7-tetrahydro-thieno[3,2-c]pyridin-3-yl]-(4-methoxy-phenyl)-methanone

There total 3 articles about [2-Butyl-5-(2-chloro-benzyl)-4,5,6,7-tetrahydro-thieno[3,2-c]pyridin-3-yl]-(4-methoxy-phenyl)-methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: 100-07-2
4-methoxy-benzoyl chloride

: 790615-52-0
2-Butyl-5-(2-chloro-benzyl)-4,5,6,7-tetrahydro-thieno[3,2-c]pyridine

: 749805-59-2
[2-Butyl-5-(2-chloro-benzyl)-4,5,6,7-tetrahydro-thieno[3,2-c]pyridin-3-yl]-(4-methoxy-phenyl)-methanone

Guidance literature:: With tin(IV) chloride; In dichloromethane; for 20h; Ambient temperature;

Reference yield:

: 55142-85-3
ticlopidine

: 749805-59-2
[2-Butyl-5-(2-chloro-benzyl)-4,5,6,7-tetrahydro-thieno[3,2-c]pyridin-3-yl]-(4-methoxy-phenyl)-methanone

Guidance literature:: Multi-step reaction with 3 steps

1: 75 percent / SnCl₄ / CH₂Cl₂ / Ambient temperature

2: 75 percent / NaBH₄, trifluoroacetic acid / CH₂Cl₂ / 3 h / Ambient temperature

3: 42 percent / SnCl₄ / CH₂Cl₂ / 20 h / Ambient temperature

With sodium tetrahydroborate; tin(IV) chloride; trifluoroacetic acid; In dichloromethane;

Reference yield:

: 90997-29-8
1-[5-(2-Chloro-benzyl)-4,5,6,7-tetrahydro-thieno[3,2-c]pyridin-2-yl]-butan-1-one

: 749805-59-2
[2-Butyl-5-(2-chloro-benzyl)-4,5,6,7-tetrahydro-thieno[3,2-c]pyridin-3-yl]-(4-methoxy-phenyl)-methanone

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / NaBH₄, trifluoroacetic acid / CH₂Cl₂ / 3 h / Ambient temperature

2: 42 percent / SnCl₄ / CH₂Cl₂ / 20 h / Ambient temperature

With sodium tetrahydroborate; tin(IV) chloride; trifluoroacetic acid; In dichloromethane;