ethyl (E)-5-(2-tert-butyldimethylsilyloxymethylphenyl)-2-methylpent-2-enoate

Base Information

Chemical Name:ethyl (E)-5-(2-tert-butyldimethylsilyloxymethylphenyl)-2-methylpent-2-enoate
CAS No.:147377-72-8
Molecular Formula:C₂₁H₃₄O₃Si
Molecular Weight:362.585
Hs Code.:

Synonyms:ethyl (E)-5-(2-tert-butyldimethylsilyloxymethylphenyl)-2-methylpent-2-enoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ethyl (E)-5-(2-tert-butyldimethylsilyloxymethylphenyl)-2-methylpent-2-enoate

Chemical Property:

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Technology Process of ethyl (E)-5-(2-tert-butyldimethylsilyloxymethylphenyl)-2-methylpent-2-enoate

There total 6 articles about ethyl (E)-5-(2-tert-butyldimethylsilyloxymethylphenyl)-2-methylpent-2-enoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 147377-70-6
3-(2-tert-butyldimethylsilyloxymethylphenyl)propanal

: 21382-82-1
(carbethoxyethylidene)triphenylphosphorane

: 147377-72-8
ethyl (E)-5-(2-tert-butyldimethylsilyloxymethylphenyl)-2-methylpent-2-enoate

Guidance literature:: In benzene; for 1h; Heating;

Reference yield:

: 87-41-2
2-benzofuran-1(3H)-one

: 147377-72-8
ethyl (E)-5-(2-tert-butyldimethylsilyloxymethylphenyl)-2-methylpent-2-enoate

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) DIBAH / 1.) toluene, -78 deg C, 1.5 h, 2.) toluene, benzene, 70 deg C, 2 h

2: 94 percent / imidazole, 4-dimethylaminopyridine / CH₂Cl₂ / 2.5 h / Ambient temperature

3: H₂ / 10percent Pd/C / ethanol / 11 h / Ambient temperature

4: DIBAH / CH₂Cl₂; hexane; 1,2-dimethoxy-ethane / 0.25 h / -78 °C

5: 87 percent / benzene / 1 h / Heating

With 1H-imidazole; dmap; hydrogen; diisobutylaluminium hydride; palladium on activated charcoal; In 1,2-dimethoxyethane; ethanol; hexane; dichloromethane; benzene;

Reference yield:

: 18162-48-6
tert-butyldimethylsilyl chloride

: 147377-72-8
ethyl (E)-5-(2-tert-butyldimethylsilyloxymethylphenyl)-2-methylpent-2-enoate

Guidance literature:: Multi-step reaction with 4 steps

1: 94 percent / imidazole, 4-dimethylaminopyridine / CH₂Cl₂ / 2.5 h / Ambient temperature

2: H₂ / 10percent Pd/C / ethanol / 11 h / Ambient temperature

3: DIBAH / CH₂Cl₂; hexane; 1,2-dimethoxy-ethane / 0.25 h / -78 °C

4: 87 percent / benzene / 1 h / Heating

With 1H-imidazole; dmap; hydrogen; diisobutylaluminium hydride; palladium on activated charcoal; In 1,2-dimethoxyethane; ethanol; hexane; dichloromethane; benzene;