ethyl 4-[(3-aminopyridin-2-yl)amino]-N-(tert-butoxycarbonyl)-L-phenylalaninate

Base Information

Chemical Name:ethyl 4-[(3-aminopyridin-2-yl)amino]-N-(tert-butoxycarbonyl)-L-phenylalaninate
CAS No.:1031337-86-6
Molecular Formula:C₂₁H₂₈N₄O₄
Molecular Weight:400.478
Hs Code.:

Synonyms:ethyl 4-[(3-aminopyridin-2-yl)amino]-N-(tert-butoxycarbonyl)-L-phenylalaninate

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Chemical Property of ethyl 4-[(3-aminopyridin-2-yl)amino]-N-(tert-butoxycarbonyl)-L-phenylalaninate

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Technology Process of ethyl 4-[(3-aminopyridin-2-yl)amino]-N-(tert-butoxycarbonyl)-L-phenylalaninate

There total 1 articles about ethyl 4-[(3-aminopyridin-2-yl)amino]-N-(tert-butoxycarbonyl)-L-phenylalaninate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1031337-78-6
ethyl N-(tert-butoxycarbonyl)-4-[(3-nitropyridin-2-yl)amino]-L-phenylalaninate

: 1031337-86-6
ethyl 4-[(3-aminopyridin-2-yl)amino]-N-(tert-butoxycarbonyl)-L-phenylalaninate

Guidance literature:: With hydrogen; palladium 10% on activated carbon; In ethanol; for 2h; under 760.051 Torr;

Reference yield: 72.0%

: 1031337-86-6
ethyl 4-[(3-aminopyridin-2-yl)amino]-N-(tert-butoxycarbonyl)-L-phenylalaninate

: 5239-82-7
cyclopropylacetic acid

: ethyl 4-[2-(cyclopropylmethyl)-3H-imidazo[4,5-b]pyridin-3-yl]-L-phenylalaninate hydrochloride

Guidance literature:: ethyl 4-[(3-aminopyridin-2-yl)amino]-N-(tert-butoxycarbonyl)-L-phenylalaninate; cyclopropylacetic acid; With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; for 18h;

With acetic acid; at 130 ℃; for 0.166667h; Microwave irradiation;

With hydrogenchloride; trifluoroacetic acid; more than 3 stages;

Reference yield: 50.0%

: 1031337-86-6
ethyl 4-[(3-aminopyridin-2-yl)amino]-N-(tert-butoxycarbonyl)-L-phenylalaninate

: 28697-11-2
(S)-1-(carbobenzyloxy)-2-piperidinecarboxylic acid

: 1031339-24-8
ethyl 4-(2-{(2S)-1-[(benzyloxy)carbonyl]piperidin-2-yl}-3H-imidazo[4,5-b]pyridin-3-yl)-N-(tert-butoxycarbonyl)-L-phenylalaninate

Guidance literature:: ethyl 4-[(3-aminopyridin-2-yl)amino]-N-(tert-butoxycarbonyl)-L-phenylalaninate; (S)-1-(carbobenzyloxy)-2-piperidinecarboxylic acid; With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃; for 20h;

With acetic acid; In ethanol; at 160 ℃; for 0.216667h; Microwave irradiation;

With water; sodium hydrogencarbonate; In dichloromethane;