ethyl 4-(2-{(2S)-1-[(benzyloxy)carbonyl]piperidin-2-yl}-3H-imidazo[4,5-b]pyridin-3-yl)-N-(tert-butoxycarbonyl)-L-phenylalaninate

Base Information

Chemical Name:ethyl 4-(2-{(2S)-1-[(benzyloxy)carbonyl]piperidin-2-yl}-3H-imidazo[4,5-b]pyridin-3-yl)-N-(tert-butoxycarbonyl)-L-phenylalaninate
CAS No.:1031339-24-8
Molecular Formula:C₃₅H₄₁N₅O₆
Molecular Weight:627.74
Hs Code.:

Synonyms:ethyl 4-(2-{(2S)-1-[(benzyloxy)carbonyl]piperidin-2-yl}-3H-imidazo[4,5-b]pyridin-3-yl)-N-(tert-butoxycarbonyl)-L-phenylalaninate

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Chemical Property of ethyl 4-(2-{(2S)-1-[(benzyloxy)carbonyl]piperidin-2-yl}-3H-imidazo[4,5-b]pyridin-3-yl)-N-(tert-butoxycarbonyl)-L-phenylalaninate

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Technology Process of ethyl 4-(2-{(2S)-1-[(benzyloxy)carbonyl]piperidin-2-yl}-3H-imidazo[4,5-b]pyridin-3-yl)-N-(tert-butoxycarbonyl)-L-phenylalaninate

There total 2 articles about ethyl 4-(2-{(2S)-1-[(benzyloxy)carbonyl]piperidin-2-yl}-3H-imidazo[4,5-b]pyridin-3-yl)-N-(tert-butoxycarbonyl)-L-phenylalaninate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 1031337-86-6
ethyl 4-[(3-aminopyridin-2-yl)amino]-N-(tert-butoxycarbonyl)-L-phenylalaninate

: 28697-11-2
(S)-1-(carbobenzyloxy)-2-piperidinecarboxylic acid

: 1031339-24-8
ethyl 4-(2-{(2S)-1-[(benzyloxy)carbonyl]piperidin-2-yl}-3H-imidazo[4,5-b]pyridin-3-yl)-N-(tert-butoxycarbonyl)-L-phenylalaninate

Guidance literature:: ethyl 4-[(3-aminopyridin-2-yl)amino]-N-(tert-butoxycarbonyl)-L-phenylalaninate; (S)-1-(carbobenzyloxy)-2-piperidinecarboxylic acid; With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃; for 20h;

With acetic acid; In ethanol; at 160 ℃; for 0.216667h; Microwave irradiation;

With water; sodium hydrogencarbonate; In dichloromethane;

Reference yield:

: C₃₅H₄₃N₅O₇

: 1031339-24-8
ethyl 4-(2-{(2S)-1-[(benzyloxy)carbonyl]piperidin-2-yl}-3H-imidazo[4,5-b]pyridin-3-yl)-N-(tert-butoxycarbonyl)-L-phenylalaninate

Guidance literature:: C₃₅H₄₃N₅O₇; With acetic acid; In ethanol; at 160 ℃; for 0.216667h; Microwave irradiation;

With sodium hydrogencarbonate; In ethanol; dichloromethane; water;

Reference yield: 100.0%

: 1031339-24-8
ethyl 4-(2-{(2S)-1-[(benzyloxy)carbonyl]piperidin-2-yl}-3H-imidazo[4,5-b]pyridin-3-yl)-N-(tert-butoxycarbonyl)-L-phenylalaninate

: 1031339-39-5
ethyl 4-(2-{(2S)-1-[(benzyloxy)carbonyl]piperidin-2-yl}-3H-imidazo[4,5-b]pyridin-3-yl)-L-phenylalaninate

Guidance literature:: ethyl 4-(2-{(2S)-1-[(benzyloxy)carbonyl]piperidin-2-yl}-3H-imidazo[4,5-b]pyridin-3-yl)-N-(tert-butoxycarbonyl)-L-phenylalaninate; With trifluoroacetic acid; In dichloromethane; at 0 - 20 ℃; for 20.1667h;

With sodium hydrogencarbonate; In water; ethyl acetate;