5-methyl-3-phenyl-5-((2,2,6,6-tetramethylpiperidin-1-yl)oxymethyl)-4,5-dihydroisoxazole

Base Information

Chemical Name:5-methyl-3-phenyl-5-((2,2,6,6-tetramethylpiperidin-1-yl)oxymethyl)-4,5-dihydroisoxazole
CAS No.:1403477-95-1
Molecular Formula:C₂₀H₃₀N₂O₂
Molecular Weight:330.47
Hs Code.:

Synonyms:5-methyl-3-phenyl-5-((2,2,6,6-tetramethylpiperidin-1-yl)oxymethyl)-4,5-dihydroisoxazole

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Chemical Property of 5-methyl-3-phenyl-5-((2,2,6,6-tetramethylpiperidin-1-yl)oxymethyl)-4,5-dihydroisoxazole

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Technology Process of 5-methyl-3-phenyl-5-((2,2,6,6-tetramethylpiperidin-1-yl)oxymethyl)-4,5-dihydroisoxazole

There total 3 articles about 5-methyl-3-phenyl-5-((2,2,6,6-tetramethylpiperidin-1-yl)oxymethyl)-4,5-dihydroisoxazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 2564-83-2,45842-10-2,126517-51-9,25657-03-8,26933-82-4,54637-06-8,64104-42-3
2,2,6,6-Tetramethyl-1-piperidinyloxy free radical

: 68843-68-5
1-phenyl-3-methyl-but-3-en-1-one oxime

: 1403477-95-1
5-methyl-3-phenyl-5-((2,2,6,6-tetramethylpiperidin-1-yl)oxymethyl)-4,5-dihydroisoxazole

Guidance literature:: With diethylazodicarboxylate; In toluene; at 50 ℃; for 15h; Inert atmosphere;
DOI:10.1002/anie.201203799

Reference yield:

: 100-52-7
benzaldehyde

: 1403477-95-1
5-methyl-3-phenyl-5-((2,2,6,6-tetramethylpiperidin-1-yl)oxymethyl)-4,5-dihydroisoxazole

Guidance literature:: Multi-step reaction with 4 steps

1: indium / tetrahydrofuran; water / 20 °C

2: Jones reagent / diethyl ether / 1 h / 0 - 20 °C

3: hydroxylamine hydrochloride; sodium acetate / ethanol; water / 20 °C

4: diethylazodicarboxylate / toluene / 15 h / 50 °C / Inert atmosphere

With indium; Jones reagent; hydroxylamine hydrochloride; sodium acetate; diethylazodicarboxylate; In tetrahydrofuran; diethyl ether; ethanol; water; toluene;
DOI:10.1002/anie.201203799

Reference yield:

: 52813-35-1
3-methyl-1-phenylbut-3-en-1-one

: 1403477-95-1
5-methyl-3-phenyl-5-((2,2,6,6-tetramethylpiperidin-1-yl)oxymethyl)-4,5-dihydroisoxazole

Guidance literature:: Multi-step reaction with 2 steps

1: hydroxylamine hydrochloride; sodium acetate / ethanol; water / 20 °C

2: diethylazodicarboxylate / toluene / 15 h / 50 °C / Inert atmosphere

With hydroxylamine hydrochloride; sodium acetate; diethylazodicarboxylate; In ethanol; water; toluene;
DOI:10.1002/anie.201203799