tert-butyl(((1R,2S,5R)-2-isopropyl-5-methylcyclohexyl)oxy)dimethylsilane

Base Information

Chemical Name:tert-butyl(((1R,2S,5R)-2-isopropyl-5-methylcyclohexyl)oxy)dimethylsilane
CAS No.:76358-81-1
Molecular Formula:C₁₆H₃₄OSi
Molecular Weight:270.531
Hs Code.:

Synonyms:tert-butyl(((1R,2S,5R)-2-isopropyl-5-methylcyclohexyl)oxy)dimethylsilane

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Chemical Property of tert-butyl(((1R,2S,5R)-2-isopropyl-5-methylcyclohexyl)oxy)dimethylsilane

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Technology Process of tert-butyl(((1R,2S,5R)-2-isopropyl-5-methylcyclohexyl)oxy)dimethylsilane

There total 11 articles about tert-butyl(((1R,2S,5R)-2-isopropyl-5-methylcyclohexyl)oxy)dimethylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 2216-51-5
(-)-menthol

: 18162-48-6
tert-butyldimethylsilyl chloride

: 76358-81-1
tert-butyl(((1R,2S,5R)-2-isopropyl-5-methylcyclohexyl)oxy)dimethylsilane

Guidance literature:: With 4-methylpyridine-1-oxide; In dichloromethane; at 20 ℃; for 24h; Molecular sieve;
DOI:10.1016/j.tetlet.2015.12.114

Reference yield: 90.0%

: 2216-51-5
(-)-menthol

: 76358-81-1
tert-butyl(((1R,2S,5R)-2-isopropyl-5-methylcyclohexyl)oxy)dimethylsilane

Guidance literature:: (-)-menthol; With sodium hydride; In tetrahydrofuran; at 0 ℃; for 1h;

t-BuMe₂Si-X; In tetrahydrofuran; at 0 ℃;
DOI:10.1021/ol049135q

Reference yield: 47.0%

: 2216-51-5
(-)-menthol

: 29681-57-0
tert-butyldimethylsilane

: 76358-81-1
tert-butyl(((1R,2S,5R)-2-isopropyl-5-methylcyclohexyl)oxy)dimethylsilane

Guidance literature:: With DARCO Charcoal supported palladium; In dibutyl ether; at 100 ℃; for 42h; Sealed tube; Glovebox; Inert atmosphere;
DOI:10.1002/chem.201803989