4'-[3,5-bis-(3,5-bis-benzyloxy-benzyloxy)-benzyloxy]-[2,2';6',2'']terpyridine

Base Information

Chemical Name:4'-[3,5-bis-(3,5-bis-benzyloxy-benzyloxy)-benzyloxy]-[2,2';6',2'']terpyridine
CAS No.:779332-28-4
Molecular Formula:C₆₄H₅₃N₃O₇
Molecular Weight:976.141
Hs Code.:

Synonyms:4'-[3,5-bis-(3,5-bis-benzyloxy-benzyloxy)-benzyloxy]-[2,2';6',2'']terpyridine

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Chemical Property of 4'-[3,5-bis-(3,5-bis-benzyloxy-benzyloxy)-benzyloxy]-[2,2';6',2'']terpyridine

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Technology Process of 4'-[3,5-bis-(3,5-bis-benzyloxy-benzyloxy)-benzyloxy]-[2,2';6',2'']terpyridine

There total 1 articles about 4'-[3,5-bis-(3,5-bis-benzyloxy-benzyloxy)-benzyloxy]-[2,2';6',2'']terpyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 101003-65-0
4'-hydroxy-2,2':6',2''-terpyridine

: 246512-25-4
methanesulfonic acid 3,5-bis-(3,5-bis-benzyloxy-benzyloxy)-benzyl ester

: 779332-28-4
4'-[3,5-bis-(3,5-bis-benzyloxy-benzyloxy)-benzyloxy]-[2,2';6',2'']terpyridine

Guidance literature:: 4'-hydroxy-2,2':6',2''-terpyridine; With potassium carbonate; In acetone; for 0.5h; Heating;

methanesulfonic acid 3,5-bis-(3,5-bis-benzyloxy-benzyloxy)-benzyl ester; In acetone; for 40h; Further stages.; Heating;
DOI:10.1039/b408605h

Reference yield: 90.0%

: ammonium hexafluorophosphate

: iron(II) chloride tetrahydrate

: 779332-28-4
4'-[3,5-bis-(3,5-bis-benzyloxy-benzyloxy)-benzyloxy]-[2,2';6',2'']terpyridine

: (Fe(N₃C₁₅H₁₀OCH₂C₆H₃(OCH₂C₆H₃(OCH₂C₆H₅)2)2)2)⁽²⁺⁾*2PF₆^(1-)*2H₂O=(Fe(N₃C₁₅H₁₀OCH₂C₆H₃(OCH₂C₆H₃(OCH₂C₆H₅)2)2)2)(PF₆)2*2H₂O

Guidance literature:: In methanol; chloroform; FeCl2*4H2O was added to boiling soln. ligand in MeOH-CHCl3 and refluxed for 2 h, soln. NH4PF6 in MeOH was added; ppt. was filtered and washed with MeOH; elem. anal.;
DOI:10.1039/b408605h

Reference yield: 76.0%

: ammonium hexafluorophosphate

: cobalt(II) chloride tetrahydrate

: 779332-28-4
4'-[3,5-bis-(3,5-bis-benzyloxy-benzyloxy)-benzyloxy]-[2,2';6',2'']terpyridine

: (Co(N₃C₁₅H₁₀OCH₂C₆H₃(OCH₂C₆H₃(OCH₂C₆H₅)2)2)2)⁽²⁺⁾*2PF₆^(1-)=(Co(N₃C₁₅H₁₀OCH₂C₆H₃(OCH₂C₆H₃(OCH₂C₆H₅)2)2)2)(PF₆)2

Guidance literature:: In methanol; ethanol; chloroform; CoCl2*4H2O was added to boiling soln. ligand in MeOH-CHCl3 and refluxed for 2 h, soln. NH4PF6 in EtOH was added; chromy. on silica (H2O, MeCN, aq. KNO3);
DOI:10.1039/b408605h