1,3-bis-benzylsalicyloyl-5-diallylbarbituric acid

Base Information

• Chemical Name: 1,3-bis-benzylsalicyloyl-5-diallylbarbituric acid
• CAS No.: 75565-51-4
• Molecular Formula: C₃₈H₃₂N₂O₇
• Molecular Weight: 628.681
• Mol file: 75565-51-4.mol

Synonyms:1,3-bis-benzylsalicyloyl-5-diallylbarbituric acid

Chemical Property of 1,3-bis-benzylsalicyloyl-5-diallylbarbituric acid

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of 1,3-bis-benzylsalicyloyl-5-diallylbarbituric acid

There total 1 articles about 1,3-bis-benzylsalicyloyl-5-diallylbarbituric acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 22.0%

2-benzyloxybenzoyl chloride (4349-62-6) + 2Ag(1+)*C10H10N2O3(2-)=Ag2C10H10N2O3 → 1,3-bis-benzylsalicyloyl-5-diallylbarbituric acid (75565-51-4)

Guidance literature:

In benzene; for 22h; boiled;

Reference yield:

1,3-bis-benzylsalicyloyl-5-diallylbarbituric acid (75565-51-4) → 5,5-dipropylbarbituric acid (2217-08-5)

Guidance literature:

Multi-step reaction with 2 steps

1: hydrogen / PdO / tetrahydrofuran

2: palladium paper / 0.08 h / 200 - 205 °C

With hydrogen; palladium; trimethyleneglycol; In tetrahydrofuran;

Reference yield:

1,3-bis-benzylsalicyloyl-5-diallylbarbituric acid (75565-51-4) → 1,3-bis-salicyloyl-5,5-dipropylbarbituric acid (75565-54-7)

Guidance literature:

With hydrogen; trimethyleneglycol; In tetrahydrofuran;

upstream raw materials:

2-benzyloxybenzoyl chloride

Downstream raw materials:

1,3-bis-salicyloyl-5,5-dipropylbarbituric acid

5,5-dipropylbarbituric acid