N-[dimethyl-(2,3,4,5-tetramethyl-cyclopenta-2,4-dienyl)-silanyl]-N'-phenyl-benzene-1,2-diamine

Base Information

• Chemical Name: N-[dimethyl-(2,3,4,5-tetramethyl-cyclopenta-2,4-dienyl)-silanyl]-N'-phenyl-benzene-1,2-diamine
• CAS No.: 324029-08-5
• Molecular Formula: C₂₃H₃₀N₂Si
• Molecular Weight: 362.59

Synonyms:N-[dimethyl-(2,3,4,5-tetramethyl-cyclopenta-2,4-dienyl)-silanyl]-N'-phenyl-benzene-1,2-diamine

Chemical Property of N-[dimethyl-(2,3,4,5-tetramethyl-cyclopenta-2,4-dienyl)-silanyl]-N'-phenyl-benzene-1,2-diamine

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Technology Process of N-[dimethyl-(2,3,4,5-tetramethyl-cyclopenta-2,4-dienyl)-silanyl]-N'-phenyl-benzene-1,2-diamine

There total 1 articles about N-[dimethyl-(2,3,4,5-tetramethyl-cyclopenta-2,4-dienyl)-silanyl]-N'-phenyl-benzene-1,2-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

1-(chlorodimethylsilyl)-2,3,4,5-tetramethylcyclopenta-2,4-diene (125542-03-2) + N-phenyl-1,2-benzenediamine (534-85-0) → N-[dimethyl-(2,3,4,5-tetramethyl-cyclopenta-2,4-dienyl)-silanyl]-N'-phenyl-benzene-1,2-diamine (324029-08-5)

Guidance literature:

In diethyl ether; at 20 ℃; for 6h;

DOI:10.1016/S0022-328X(00)00179-0

Reference yield: 28.0%

tetrakis(dimethylamido)zirconium (IV) (19756-04-8) + N-[dimethyl-(2,3,4,5-tetramethyl-cyclopenta-2,4-dienyl)-silanyl]-N'-phenyl-benzene-1,2-diamine (324029-08-5) → C6H4N(C6H5)NSi(CH3)2C5(CH3)4ZrCl(NH(CH3)2)2 (324029-10-9)

Guidance literature:

In hexane; a mixt. in hexane was stirred for 15 min (N2 atm.); the supernatant was removed, the solid was washed with pentane; elem. anal.;

DOI:10.1016/S0022-328X(00)00179-0

Reference yield: 25.0%

tetrakis(dimethylamido)zirconium (IV) (19756-04-8) + N-[dimethyl-(2,3,4,5-tetramethyl-cyclopenta-2,4-dienyl)-silanyl]-N'-phenyl-benzene-1,2-diamine (324029-08-5) → C6H4N(C6H5)NSi(CH3)2C5(CH3)4ZrN(CH3)2NH(CH3)2 + C6H4N(C6H5)NSi(CH3)2C5(CH3)4ZrCl(NH(CH3)2)2 (324029-10-9)

Guidance literature:

In hexane; a mixt. in hexane was stirred for 6 h (N2 atm.); ppt. was extd. with pentane, recrystd. from toluene-pentane; elem. anal.;

DOI:10.1016/S0022-328X(00)00179-0

upstream raw materials:

1-(chlorodimethylsilyl)-2,3,4,5-tetramethylcyclopenta-2,4-diene

N-phenyl-1,2-benzenediamine

Downstream raw materials:

C₆H₄N(C₆H₅)NSi(CH₃)2C₅(CH₃)4ZrCl(NH(CH₃)2)2

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