N,N'-didodecyl-4-[3-(dodecylamino)-3-oxopropyl]-4-{[(4-iodophenyl)carbonyl]amino}heptanediamide

Base Information

Chemical Name:N,N'-didodecyl-4-[3-(dodecylamino)-3-oxopropyl]-4-{[(4-iodophenyl)carbonyl]amino}heptanediamide
CAS No.:883699-95-4
Molecular Formula:C₅₃H₉₅IN₄O₄
Molecular Weight:979.266
Hs Code.:

Synonyms:N,N'-didodecyl-4-[3-(dodecylamino)-3-oxopropyl]-4-{[(4-iodophenyl)carbonyl]amino}heptanediamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N,N'-didodecyl-4-[3-(dodecylamino)-3-oxopropyl]-4-{[(4-iodophenyl)carbonyl]amino}heptanediamide

Chemical Property:

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Technology Process of N,N'-didodecyl-4-[3-(dodecylamino)-3-oxopropyl]-4-{[(4-iodophenyl)carbonyl]amino}heptanediamide

There total 2 articles about N,N'-didodecyl-4-[3-(dodecylamino)-3-oxopropyl]-4-{[(4-iodophenyl)carbonyl]amino}heptanediamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 883699-81-8
N,N'-didodecyl-4-[3-(dodecylamino)-3-oxopropyl]-4-nitroheptanediamide

: 883699-95-4
N,N'-didodecyl-4-[3-(dodecylamino)-3-oxopropyl]-4-{[(4-iodophenyl)carbonyl]amino}heptanediamide

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / Raney-Ni / ethanol / 48 h / 40 - 50 °C / 4500.36 Torr

2: Et₃N / CH₂Cl₂ / 3 h / 20 °C

With hydrogen; triethylamine; nickel; In ethanol; dichloromethane;
DOI:10.1039/b518174g

Reference yield:

: 883699-88-5
4-amino-N,N'-didodecyl-4-[3-(dodecylamino)-3-oxopropyl]heptanediamide

: 1711-02-0
4-iodobenzoic acid chloride

: 883699-95-4
N,N'-didodecyl-4-[3-(dodecylamino)-3-oxopropyl]-4-{[(4-iodophenyl)carbonyl]amino}heptanediamide

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 3h;
DOI:10.1039/b518174g

Reference yield:

: 883699-95-4
N,N'-didodecyl-4-[3-(dodecylamino)-3-oxopropyl]-4-{[(4-iodophenyl)carbonyl]amino}heptanediamide

: 1066-54-2
trimethylsilylacetylene

: 883700-01-4
N,N'-didodecyl-4-[3-(dodecylamino)-3-oxopropyl]-4-[({4-[(trimethylsilyl)ethynyl]phenyl}carbonyl)amino]heptanediamide

Guidance literature:: With copper(l) iodide; tetrabutylammomium bromide; diisopropylamine; bis-triphenylphosphine-palladium(II) chloride; In tetrahydrofuran; at 20 ℃; for 24h;
DOI:10.1039/b518174g