N,N'-didodecyl-4-[3-(dodecylamino)-3-oxopropyl]-4-[({4-[(trimethylsilyl)ethynyl]phenyl}carbonyl)amino]heptanediamide

Base Information

Chemical Name:N,N'-didodecyl-4-[3-(dodecylamino)-3-oxopropyl]-4-[({4-[(trimethylsilyl)ethynyl]phenyl}carbonyl)amino]heptanediamide
CAS No.:883700-01-4
Molecular Formula:C₅₈H₁₀₄N₄O₄Si
Molecular Weight:949.574
Hs Code.:

Synonyms:N,N'-didodecyl-4-[3-(dodecylamino)-3-oxopropyl]-4-[({4-[(trimethylsilyl)ethynyl]phenyl}carbonyl)amino]heptanediamide

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Chemical Property of N,N'-didodecyl-4-[3-(dodecylamino)-3-oxopropyl]-4-[({4-[(trimethylsilyl)ethynyl]phenyl}carbonyl)amino]heptanediamide

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Technology Process of N,N'-didodecyl-4-[3-(dodecylamino)-3-oxopropyl]-4-[({4-[(trimethylsilyl)ethynyl]phenyl}carbonyl)amino]heptanediamide

There total 3 articles about N,N'-didodecyl-4-[3-(dodecylamino)-3-oxopropyl]-4-[({4-[(trimethylsilyl)ethynyl]phenyl}carbonyl)amino]heptanediamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 883699-95-4
N,N'-didodecyl-4-[3-(dodecylamino)-3-oxopropyl]-4-{[(4-iodophenyl)carbonyl]amino}heptanediamide

: 1066-54-2
trimethylsilylacetylene

: 883700-01-4
N,N'-didodecyl-4-[3-(dodecylamino)-3-oxopropyl]-4-[({4-[(trimethylsilyl)ethynyl]phenyl}carbonyl)amino]heptanediamide

Guidance literature:: With copper(l) iodide; tetrabutylammomium bromide; diisopropylamine; bis-triphenylphosphine-palladium(II) chloride; In tetrahydrofuran; at 20 ℃; for 24h;
DOI:10.1039/b518174g

Reference yield:

: 883699-88-5
4-amino-N,N'-didodecyl-4-[3-(dodecylamino)-3-oxopropyl]heptanediamide

: 883700-01-4
N,N'-didodecyl-4-[3-(dodecylamino)-3-oxopropyl]-4-[({4-[(trimethylsilyl)ethynyl]phenyl}carbonyl)amino]heptanediamide

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / CH₂Cl₂ / 3 h / 20 °C

2: 978 mg / i-Pr₂NH; CuI; (n-Bu)4NBr / [Pd(PPh₃)2Cl₂] / tetrahydrofuran / 24 h / 20 °C

With copper(l) iodide; tetrabutylammomium bromide; triethylamine; diisopropylamine; bis-triphenylphosphine-palladium(II) chloride; In tetrahydrofuran; dichloromethane;
DOI:10.1039/b518174g

Reference yield:

: 883699-81-8
N,N'-didodecyl-4-[3-(dodecylamino)-3-oxopropyl]-4-nitroheptanediamide

: 883700-01-4
N,N'-didodecyl-4-[3-(dodecylamino)-3-oxopropyl]-4-[({4-[(trimethylsilyl)ethynyl]phenyl}carbonyl)amino]heptanediamide

Guidance literature:: Multi-step reaction with 3 steps

1: H₂ / Raney-Ni / ethanol / 48 h / 40 - 50 °C / 4500.36 Torr

2: Et₃N / CH₂Cl₂ / 3 h / 20 °C

3: 978 mg / i-Pr₂NH; CuI; (n-Bu)4NBr / [Pd(PPh₃)2Cl₂] / tetrahydrofuran / 24 h / 20 °C

With copper(l) iodide; tetrabutylammomium bromide; hydrogen; triethylamine; diisopropylamine; bis-triphenylphosphine-palladium(II) chloride; nickel; In tetrahydrofuran; ethanol; dichloromethane;
DOI:10.1039/b518174g