Ru(2,2'-bipyridine)2(3-hydroxy-2-methyl-4-thiopyrone^(1-))PF₆*CH₂Cl₂

Base Information

Chemical Name:Ru(2,2'-bipyridine)2(3-hydroxy-2-methyl-4-thiopyrone^(1-))PF₆*CH₂Cl₂
CAS No.:1013397-31-3
Molecular Formula:CH₂Cl₂*C₂₆H₂₁N₄O₂RuS*F₆P
Molecular Weight:784.511
Hs Code.:

Ru(2,2'-bipyridine)2(3-hydroxy-2-methyl-4-thiopyrone<sup>(1-)</sup>)PF<sub>6</sub>*CH<sub>2</sub>Cl<sub>2</sub>

Synonyms:Ru(2,2'-bipyridine)2(3-hydroxy-2-methyl-4-thiopyrone^(1-))PF₆*CH₂Cl₂

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Ru(2,2'-bipyridine)2(3-hydroxy-2-methyl-4-thiopyrone^(1-))PF₆*CH₂Cl₂

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Technology Process of Ru(2,2'-bipyridine)2(3-hydroxy-2-methyl-4-thiopyrone^(1-))PF₆*CH₂Cl₂

There total 1 articles about Ru(2,2'-bipyridine)2(3-hydroxy-2-methyl-4-thiopyrone^(1-))PF₆*CH₂Cl₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 17084-13-8
potassium hexafluorophosphate

: cis-dichloro(2,2′-bipyridine)ruthenium(II)chloride

: 23060-85-7
3-hydroxy-2-methylpyran-4(1H)-thione

: 75-09-2
dichloromethane

: 1013397-31-3
Ru(2,2'-bipyridine)2(3-hydroxy-2-methyl-4-thiopyrone^(1-))PF₆*CH₂Cl₂

Guidance literature:: In ethylene glycol; (under N2, Schlenk); Ru-complex and ligand mixed with ethylene glycol, brought to 130°C, stirred for 45 min, poured into H2O, KPF6 added; vac. filtered, basic alumina column with CH2Cl2/MeCN, crystd. in CH2Cl2/Et2O; elem. anal.;
DOI:10.1021/ic7021962