4-(4'-(di-(4-methoxyphenyl)amino)phenyl)-N-(2-ethylhexyl)-1,8-naphthalimide

Base Information

Chemical Name:4-(4'-(di-(4-methoxyphenyl)amino)phenyl)-N-(2-ethylhexyl)-1,8-naphthalimide
CAS No.:1605305-91-6
Molecular Formula:C₄₀H₄₀N₂O₄
Molecular Weight:612.769
Hs Code.:

Synonyms:4-(4'-(di-(4-methoxyphenyl)amino)phenyl)-N-(2-ethylhexyl)-1,8-naphthalimide

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Chemical Property of 4-(4'-(di-(4-methoxyphenyl)amino)phenyl)-N-(2-ethylhexyl)-1,8-naphthalimide

Chemical Property:

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Technology Process of 4-(4'-(di-(4-methoxyphenyl)amino)phenyl)-N-(2-ethylhexyl)-1,8-naphthalimide

There total 6 articles about 4-(4'-(di-(4-methoxyphenyl)amino)phenyl)-N-(2-ethylhexyl)-1,8-naphthalimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 875667-84-8
4-methoxy-N-(4-methoxyphenyl)-N-[4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]benzenamine

: 1193092-32-8
6-bromo-2-(2-ethylhexyl)-1H-benzo[de]isoquinoline-1,3(2H)-dione

: 1605305-91-6
4-(4'-(di-(4-methoxyphenyl)amino)phenyl)-N-(2-ethylhexyl)-1,8-naphthalimide

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; potassium carbonate; In tetrahydrofuran; water; at 80 ℃; for 24h; Inert atmosphere;
DOI:10.1016/j.dyepig.2014.02.023

Reference yield:

: 194416-45-0
4-bromo-N,N-bis-(4-methoxyphenyl)aniline

: 1605305-91-6
4-(4'-(di-(4-methoxyphenyl)amino)phenyl)-N-(2-ethylhexyl)-1,8-naphthalimide

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium / tetrahydrofuran / -78 - 20 °C

1.2: 24 h

2.1: bis-triphenylphosphine-palladium(II) chloride; potassium carbonate / tetrahydrofuran; water / 24 h / 80 °C / Inert atmosphere

With bis-triphenylphosphine-palladium(II) chloride; n-butyllithium; potassium carbonate; In tetrahydrofuran; water; 2.1: |Suzuki Coupling;
DOI:10.1016/j.dyepig.2014.02.023

Reference yield:

: 696-62-8
para-iodoanisole

: 1605305-91-6
4-(4'-(di-(4-methoxyphenyl)amino)phenyl)-N-(2-ethylhexyl)-1,8-naphthalimide

Guidance literature:: Multi-step reaction with 3 steps

1.1: 1,10-Phenanthroline; copper(l) chloride; potassium hydroxide / para-xylene / 180 °C

2.1: n-butyllithium / tetrahydrofuran / -78 - 20 °C

2.2: 24 h

3.1: bis-triphenylphosphine-palladium(II) chloride; potassium carbonate / tetrahydrofuran; water / 24 h / 80 °C / Inert atmosphere

With bis-triphenylphosphine-palladium(II) chloride; n-butyllithium; 1,10-Phenanthroline; potassium carbonate; copper(l) chloride; potassium hydroxide; In tetrahydrofuran; para-xylene; water; 1.1: |Ullmann Condensation / 3.1: |Suzuki Coupling;
DOI:10.1016/j.dyepig.2014.02.023