BenzenaMine, N,N-bis(4-Methoxyphenyl)-4-(4,4,5,5-tetraMethyl-1,3,2-dioxaborolan-2-yl)-

Base Information

• Chemical Name: BenzenaMine, N,N-bis(4-Methoxyphenyl)-4-(4,4,5,5-tetraMethyl-1,3,2-dioxaborolan-2-yl)-
• CAS No.: 875667-84-8
• Molecular Formula: C₂₆H₃₀BNO₄
• Molecular Weight: 431.339
• Mol file: 875667-84-8.mol

Synonyms:

Chemical Property of BenzenaMine, N,N-bis(4-Methoxyphenyl)-4-(4,4,5,5-tetraMethyl-1,3,2-dioxaborolan-2-yl)-

Chemical Property:

• Boiling Point: 565.4±45.0 °C(Predicted)
• PKA: -2.02±0.60(Predicted)
• PSA: 40.16000
• Density: 1.15±0.1 g/cm3(Predicted)
• LogP: 5.47280
• Storage Temp.: under inert gas (nitrogen or Argon) at 2-8°C

Purity/Quality:

99%, ^*data from raw suppliers

4-Methoxy-N-(4-methoxyphenyl)-N-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)aniline 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of BenzenaMine, N,N-bis(4-Methoxyphenyl)-4-(4,4,5,5-tetraMethyl-1,3,2-dioxaborolan-2-yl)-

There total 17 articles about BenzenaMine, N,N-bis(4-Methoxyphenyl)-4-(4,4,5,5-tetraMethyl-1,3,2-dioxaborolan-2-yl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

2,3-dimethyl-2,3-butane diol (76-09-5) + Triisopropyl borate (5419-55-6) + 4-bromo-N,N-bis-(4-methoxyphenyl)aniline (194416-45-0) → 4-methoxy-N-(4-methoxyphenyl)-N-[4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]benzenamine (875667-84-8)

Guidance literature:

4-bromo-N,N-bis-(4-methoxyphenyl)aniline; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.5h; Schlenk technique; Inert atmosphere;

Triisopropyl borate; In tetrahydrofuran; hexane; at -78 ℃; for 0.166667h; Schlenk technique; Inert atmosphere;

2,3-dimethyl-2,3-butane diol; In tetrahydrofuran; hexane; at 20 ℃; for 69h; Schlenk technique; Inert atmosphere;

DOI:10.1002/chem.202102052

Reference yield: 92.0%

bis(pinacol)diborane (73183-34-3) + 4-bromo-N,N-bis-(4-methoxyphenyl)aniline (194416-45-0) → 4-methoxy-N-(4-methoxyphenyl)-N-[4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]benzenamine (875667-84-8)

Guidance literature:

With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate; In 1,4-dioxane;

DOI:10.1002/cjoc.202100022

Reference yield: 81.0%

4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane (25015-63-8) + 4-bromo-N,N-bis-(4-methoxyphenyl)aniline (194416-45-0) → 4-methoxy-N-(4-methoxyphenyl)-N-[4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]benzenamine (875667-84-8)

Guidance literature:

With bis-triphenylphosphine-palladium(II) chloride; triethylamine; In toluene; at 110 ℃; for 15h; Darkness;

DOI:10.1055/s-0034-1378818

upstream raw materials:

para-iodoanisole

4-bromo-aniline

bis(pinacol)diborane

4-bromo-N,N-bis-(4-methoxyphenyl)aniline

Downstream raw materials:

C₅₉H₅₂BF₆NO₂S₂

C₆₀H₅₄N₂O₈S₃

4-(4'-(di-(4-methoxyphenyl)amino)phenyl)-N-(2-ethylhexyl)-1,8-naphthalimide

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