5-[(2-methyl-1H-benzimidazol-1-yl)methyl]-4-(4-methylphenyl)-4H-1,2,4-triazol-3-yl hydrosulfide

Base Information

Chemical Name:5-[(2-methyl-1H-benzimidazol-1-yl)methyl]-4-(4-methylphenyl)-4H-1,2,4-triazol-3-yl hydrosulfide
CAS No.:343977-51-5
Molecular Formula:C₁₈H₁₇N₅S
Molecular Weight:335.432
Hs Code.:
Mol file:343977-51-5.mol

Synonyms:1-[(4-(4'-methylphenyl)-3-thioxy-4H-1,2,4-triazol-5-yl)methyl]-2-methyl-1H-benzimidazoles

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Chemical Property of 5-[(2-methyl-1H-benzimidazol-1-yl)methyl]-4-(4-methylphenyl)-4H-1,2,4-triazol-3-yl hydrosulfide

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Technology Process of 5-[(2-methyl-1H-benzimidazol-1-yl)methyl]-4-(4-methylphenyl)-4H-1,2,4-triazol-3-yl hydrosulfide

There total 7 articles about 5-[(2-methyl-1H-benzimidazol-1-yl)methyl]-4-(4-methylphenyl)-4H-1,2,4-triazol-3-yl hydrosulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 343977-49-1
4-(4'-methylphenyl)-1-[1-carbonylmethyl-(2-methyl-1H-benzimidazole)]-thiosemicarbazide

: 343977-51-5
1-[(4-(4'-methylphenyl)-3-thioxy-4H-1,2,4-triazol-5-yl)methyl]-2-methyl-1H-benzimidazoles

Guidance literature:: With sodium hydroxide; for 1h; Heating;

Reference yield: 56.4%

: 97420-40-1
2-(2-methyl-1H-benzimidazol-1-yl)acetohydrazide

: 622-59-3
1-isothiocyanato-4-methylbenzene

: 343977-51-5
1-[(4-(4'-methylphenyl)-3-thioxy-4H-1,2,4-triazol-5-yl)methyl]-2-methyl-1H-benzimidazoles

Guidance literature:: 2-(2-methyl-1H-benzimidazol-1-yl)acetohydrazide; 1-isothiocyanato-4-methylbenzene; In ethanol; for 1h; Reflux;

With sodium hydroxide; for 2h; Reflux;
DOI:10.1155/2016/1507049

Reference yield:

: 615-15-6
2-Methyl-1H-benzimidazole

: 343977-51-5
1-[(4-(4'-methylphenyl)-3-thioxy-4H-1,2,4-triazol-5-yl)methyl]-2-methyl-1H-benzimidazoles

Guidance literature:: Multi-step reaction with 4 steps

1: 95 percent / polyethylene glycol-4000; K₂CO₃ / acetone / 20 °C

2: 94 percent / 98 percent hydrazine hydrate / methanol / 3 h / Heating

3: 90 percent / ethanol / 3 h / Heating

4: 92 percent / 5 percent NaOH / 1 h / Heating

With sodium hydroxide; polyethylene glycol-4000; potassium carbonate; hydrazine hydrate; In methanol; ethanol; acetone;