{[1-(tert-Butyl-dimethyl-silanyloxy)-propa-1,2-dienyl]-dimethyl-silanyl}-benzene

Base Information

Chemical Name:{[1-(tert-Butyl-dimethyl-silanyloxy)-propa-1,2-dienyl]-dimethyl-silanyl}-benzene
CAS No.:129103-44-2
Molecular Formula:C₁₇H₂₈OSi₂
Molecular Weight:304.58
Hs Code.:

Synonyms:{[1-(tert-Butyl-dimethyl-silanyloxy)-propa-1,2-dienyl]-dimethyl-silanyl}-benzene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of {[1-(tert-Butyl-dimethyl-silanyloxy)-propa-1,2-dienyl]-dimethyl-silanyl}-benzene

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Technology Process of {[1-(tert-Butyl-dimethyl-silanyloxy)-propa-1,2-dienyl]-dimethyl-silanyl}-benzene

There total 2 articles about {[1-(tert-Butyl-dimethyl-silanyloxy)-propa-1,2-dienyl]-dimethyl-silanyl}-benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 192569-18-9
α-bromovinyldimethylphenylsilane

: 129103-44-2
{[1-(tert-Butyl-dimethyl-silanyloxy)-propa-1,2-dienyl]-dimethyl-silanyl}-benzene

Guidance literature:: Multi-step reaction with 2 steps

1: t-BuLi / tetrahydrofuran / -120 °C

2: 2.) HMPA / 1.) THF, 15 deg C, 1 atm, 1 h, 2.) -78 deg to 20 deg C

With N,N,N,N,N,N-hexamethylphosphoric triamide; tert.-butyl lithium; In tetrahydrofuran;
DOI:10.1021/ja00175a051

Reference yield:

: 201230-82-2
carbon monoxide

: 129103-40-8
C₁₀H₁₃LiSi

: 18162-48-6
tert-butyldimethylsilyl chloride

: 129103-44-2
{[1-(tert-Butyl-dimethyl-silanyloxy)-propa-1,2-dienyl]-dimethyl-silanyl}-benzene

: 129103-43-1
{[2-(tert-Butyl-dimethyl-silanyloxy)-cycloprop-1-enyl]-dimethyl-silanyl}-benzene

Guidance literature:: With N,N,N,N,N,N-hexamethylphosphoric triamide; Yield given. Multistep reaction. Yields of byproduct given; 1.) THF, 15 deg C, 1 atm, 1 h, 2.) -78 deg to 20 deg C;
DOI:10.1021/ja00175a051