ethyl 1-(O,O-diethylthiophosphoryl)-2-(o-chlorophenyl)-3-pyrroline-3-carboxylate

Base Information

Chemical Name:ethyl 1-(O,O-diethylthiophosphoryl)-2-(o-chlorophenyl)-3-pyrroline-3-carboxylate
CAS No.:1070874-81-5
Molecular Formula:C₁₇H₂₃ClNO₄PS
Molecular Weight:403.867
Hs Code.:

Synonyms:ethyl 1-(O,O-diethylthiophosphoryl)-2-(o-chlorophenyl)-3-pyrroline-3-carboxylate

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Chemical Property of ethyl 1-(O,O-diethylthiophosphoryl)-2-(o-chlorophenyl)-3-pyrroline-3-carboxylate

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Technology Process of ethyl 1-(O,O-diethylthiophosphoryl)-2-(o-chlorophenyl)-3-pyrroline-3-carboxylate

There total 1 articles about ethyl 1-(O,O-diethylthiophosphoryl)-2-(o-chlorophenyl)-3-pyrroline-3-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

: C₁₁H₁₅ClNO₂PS

: 14369-81-4
ethyl 2,3-butadienoate

: 1070874-81-5
ethyl 1-(O,O-diethylthiophosphoryl)-2-(o-chlorophenyl)-3-pyrroline-3-carboxylate

Guidance literature:: With triphenylphosphine; In dichloromethane; at 20 ℃; for 7h; atmospheric pressure;
DOI:10.1016/j.tet.2008.07.075

Reference yield: 63.0%

: 67-56-1
methanol

: 1070874-81-5
ethyl 1-(O,O-diethylthiophosphoryl)-2-(o-chlorophenyl)-3-pyrroline-3-carboxylate

: 1070874-91-7
methyl 2-(o-chlorophenyl)-3-pyrroline-3-carboxylate

: C₁₆H₁₉ClNO₄PS

Guidance literature:: methanol; ethyl 1-(O,O-diethylthiophosphoryl)-2-(o-chlorophenyl)-3-pyrroline-3-carboxylate; With hydrogenchloride; at 20 - 60 ℃; for 36h;

With triethylamine; In dichloromethane; at 20 ℃; for 1h; Further stages.;
DOI:10.1016/j.tet.2008.07.075