2,4-Dihydroxy-6-methyl-3-[(E)-3-methyl-5-((1S,2R,6R)-1,2,6-trimethyl-3-oxo-cyclohexyl)-pent-2-enyl]-benzoic acid methyl ester

Base Information

• Chemical Name: 2,4-Dihydroxy-6-methyl-3-[(E)-3-methyl-5-((1S,2R,6R)-1,2,6-trimethyl-3-oxo-cyclohexyl)-pent-2-enyl]-benzoic acid methyl ester
• CAS No.: 165187-10-0
• Molecular Formula: C₂₄H₃₄O₅
• Molecular Weight: 402.531

Synonyms:2,4-Dihydroxy-6-methyl-3-[(E)-3-methyl-5-((1S,2R,6R)-1,2,6-trimethyl-3-oxo-cyclohexyl)-pent-2-enyl]-benzoic acid methyl ester

Chemical Property of 2,4-Dihydroxy-6-methyl-3-[(E)-3-methyl-5-((1S,2R,6R)-1,2,6-trimethyl-3-oxo-cyclohexyl)-pent-2-enyl]-benzoic acid methyl ester

Chemical Property:

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Technology Process of 2,4-Dihydroxy-6-methyl-3-[(E)-3-methyl-5-((1S,2R,6R)-1,2,6-trimethyl-3-oxo-cyclohexyl)-pent-2-enyl]-benzoic acid methyl ester

There total 1 articles about 2,4-Dihydroxy-6-methyl-3-[(E)-3-methyl-5-((1S,2R,6R)-1,2,6-trimethyl-3-oxo-cyclohexyl)-pent-2-enyl]-benzoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methanol (67-56-1) + dechloro-12,13-dihydroascochlorin → 2,4-Dihydroxy-6-methyl-3-[(E)-3-methyl-5-((1S,2R,6R)-1,2,6-trimethyl-3-oxo-cyclohexyl)-pent-2-enyl]-benzoic acid methyl ester (165187-10-0)

Guidance literature:

With potassium cyanide; manganese(IV) oxide; acetic acid; 1.) room temp., overnight, 2.) 70 deg C, 6 h;

DOI:10.1021/jo961074p

Reference yield:

2,4-Dihydroxy-6-methyl-3-[(E)-3-methyl-5-((1S,2R,6R)-1,2,6-trimethyl-3-oxo-cyclohexyl)-pent-2-enyl]-benzoic acid methyl ester (165187-10-0) → (2R,3S,4R)-3-[(E)-5-(2,6-Dihydroxy-4-methyl-phenyl)-3-methyl-pent-3-enyl]-2,3,4-trimethyl-cyclohexanone

Guidance literature:

With sodium hydroxide; In tetrahydrofuran; methanol; at 70 ℃;

DOI:10.1021/jo961074p

Reference yield:

2,4-Dihydroxy-6-methyl-3-[(E)-3-methyl-5-((1S,2R,6R)-1,2,6-trimethyl-3-oxo-cyclohexyl)-pent-2-enyl]-benzoic acid methyl ester (165187-10-0) → (2R,3S,4R)-3-[2-(5-Hydroxy-8-iodo-2,7-dimethyl-chroman-2-yl)-ethyl]-2,3,4-trimethyl-cyclohexanone + 5-Hydroxy-2,7-dimethyl-2-[2-((1S,2R,6R)-1,2,6-trimethyl-3-oxo-cyclohexyl)-ethyl]-chroman-8-carboxylic acid methyl ester

Guidance literature:

With chloro-trimethyl-silane; sodium iodide; In acetonitrile; 1.) 60 deg C, 8 h, 2.) room temp., 4 d;

DOI:10.1021/jo961074p

upstream raw materials:

methanol

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