4-bromo-2,6-difluorophenethyl acetate

Base Information

Chemical Name:4-bromo-2,6-difluorophenethyl acetate
CAS No.:1426050-45-4
Molecular Formula:C₁₀H₉BrF₂O₂
Molecular Weight:279.081
Hs Code.:

Synonyms:4-bromo-2,6-difluorophenethyl acetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-bromo-2,6-difluorophenethyl acetate

Chemical Property:

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Technology Process of 4-bromo-2,6-difluorophenethyl acetate

There total 5 articles about 4-bromo-2,6-difluorophenethyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 1426050-44-3
2-(4-bromo-2,6-difluoro-phenyl)ethanol

: 108-24-7
acetic anhydride

: 1426050-45-4
4-bromo-2,6-difluorophenethyl acetate

Guidance literature:: With pyridine; dmap; In ethanol; at 20 ℃; for 72h;

Reference yield:

: 162744-60-7
5-bromo-2-(bromomethyl)-1,3-difluoro-benzene

: 1426050-45-4
4-bromo-2,6-difluorophenethyl acetate

Guidance literature:: Multi-step reaction with 5 steps

1: dimethyl sulfoxide / 3 h / 23 °C

2: sulfuric acid; acetic acid / 1 h / 100 °C

3: water; sodium hydroxide / ethanol / 80 °C

4: borane-THF / 48 h / 40 °C

5: pyridine; dmap / ethanol / 72 h / 20 °C

With pyridine; dmap; borane-THF; sulfuric acid; water; acetic acid; sodium hydroxide; In ethanol; dimethyl sulfoxide;

Reference yield:

: 537033-54-8
2-(4-bromo-2,6-difluorophenyl)acetic acid

: 1426050-45-4
4-bromo-2,6-difluorophenethyl acetate

Guidance literature:: Multi-step reaction with 2 steps

1: borane-THF / 48 h / 40 °C

2: pyridine; dmap / ethanol / 72 h / 20 °C

With pyridine; dmap; borane-THF; In ethanol;