3,6-di-O-acetyl-2-azido-1-N,4-O-dibenzyl-1,2,5-trideoxy-1,5-imino-D-glucitol

Base Information

Chemical Name:3,6-di-O-acetyl-2-azido-1-N,4-O-dibenzyl-1,2,5-trideoxy-1,5-imino-D-glucitol
CAS No.:1401914-66-6
Molecular Formula:C₂₄H₂₈N₄O₅
Molecular Weight:452.51
Hs Code.:

Synonyms:3,6-di-O-acetyl-2-azido-1-N,4-O-dibenzyl-1,2,5-trideoxy-1,5-imino-D-glucitol

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Chemical Property of 3,6-di-O-acetyl-2-azido-1-N,4-O-dibenzyl-1,2,5-trideoxy-1,5-imino-D-glucitol

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Technology Process of 3,6-di-O-acetyl-2-azido-1-N,4-O-dibenzyl-1,2,5-trideoxy-1,5-imino-D-glucitol

There total 1 articles about 3,6-di-O-acetyl-2-azido-1-N,4-O-dibenzyl-1,2,5-trideoxy-1,5-imino-D-glucitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 4-O-acetyl-5-azido-2-N,3-O-dibenzyl-2,5,6-trideoxy-2,6-imino-L-gulose acetyl methyl acetal

: 1401914-66-6
3,6-di-O-acetyl-2-azido-1-N,4-O-dibenzyl-1,2,5-trideoxy-1,5-imino-D-glucitol

Guidance literature:: 4-O-acetyl-5-azido-2-N,3-O-dibenzyl-2,5,6-trideoxy-2,6-imino-L-gulose acetyl methyl acetal; With pyridine; diisobutylaluminium hydride; In dichloromethane; at -78 ℃; for 0.666667h; Inert atmosphere;

With sodium tetrahydroborate; In methanol; at -10 ℃; for 2h; Inert atmosphere;

With acetic anhydride; at 20 ℃; for 16h; Inert atmosphere;
DOI:10.1002/chem.201200110

Reference yield: 81.0%

: 1401914-66-6
3,6-di-O-acetyl-2-azido-1-N,4-O-dibenzyl-1,2,5-trideoxy-1,5-imino-D-glucitol

: 108-24-7
acetic anhydride

: 1401914-68-8
2-acetamido-3,6-di-O-acetyl-1-N,4-O-dibenzyl-1,2,5-trideoxy-1,5-imino-D-glucitol

Guidance literature:: With copper(II) sulfate; acetic acid; zinc; In tetrahydrofuran; water; for 0.333333h; Inert atmosphere;
DOI:10.1002/chem.201200110