3,N-dicyclohexyl-N'-(4-nitro-phenyl)-[1,3]thiazetidine-2,4-diylidenediamine

Base Information

• Chemical Name: 3,N-dicyclohexyl-N'-(4-nitro-phenyl)-[1,3]thiazetidine-2,4-diylidenediamine
• CAS No.: 36908-22-2
• Molecular Formula: C₂₀H₂₆N₄O₂S
• Molecular Weight: 386.518

Synonyms:3,N-dicyclohexyl-N'-(4-nitro-phenyl)-[1,3]thiazetidine-2,4-diylidenediamine

Chemical Property of 3,N-dicyclohexyl-N'-(4-nitro-phenyl)-[1,3]thiazetidine-2,4-diylidenediamine

Chemical Property:

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Technology Process of 3,N-dicyclohexyl-N'-(4-nitro-phenyl)-[1,3]thiazetidine-2,4-diylidenediamine

There total 1 articles about 3,N-dicyclohexyl-N'-(4-nitro-phenyl)-[1,3]thiazetidine-2,4-diylidenediamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

dicyclohexyl-carbodiimide (538-75-0) + p-nitrophenyl isothiocyanate (2131-61-5) → 3,N-dicyclohexyl-N'-(4-nitro-phenyl)-[1,3]thiazetidine-2,4-diylidenediamine (36908-22-2)

Guidance literature:

DOI:10.1021/ja00765a039

Reference yield: 76.0%

3,N-dicyclohexyl-N'-(4-nitro-phenyl)-[1,3]thiazetidine-2,4-diylidenediamine (36908-22-2) + (carbethoxyethylidene)triphenylphosphorane (21382-82-1) → 1-Cyclohexyl-2-[(E)-cyclohexylimino]-3-methyl-4-[(E)-4-nitro-phenylimino]-azetidine-3-carboxylic acid ethyl ester (83324-96-3) + triphenylphosphine sulfide (3878-45-3)

Guidance literature:

In chloroform; at 45 ℃; for 96h;

DOI:10.1016/S0040-4039(00)88446-4

Reference yield: 13.0%

3,N-dicyclohexyl-N'-(4-nitro-phenyl)-[1,3]thiazetidine-2,4-diylidenediamine (36908-22-2) + diethyl 2-(triphenylphosphoranylidene)malonate (7509-48-0) → 1-Cyclohexyl-2-[(E)-cyclohexylimino]-4-[(E)-4-nitro-phenylimino]-azetidine-3,3-dicarboxylic acid diethyl ester (83324-97-4) + triphenylphosphine sulfide (3878-45-3)

Guidance literature:

In chloroform; at 45 ℃; for 336h;

DOI:10.1016/S0040-4039(00)88446-4

upstream raw materials:

dicyclohexyl-carbodiimide

p-nitrophenyl isothiocyanate

Downstream raw materials:

1-Cyclohexyl-2-[(E)-cyclohexylimino]-4-[(E)-4-nitro-phenylimino]-azetidine-3,3-dicarboxylic acid diethyl ester

triphenylphosphine sulfide

1-Cyclohexyl-2-[(E)-cyclohexylimino]-3-methyl-4-[(E)-4-nitro-phenylimino]-azetidine-3-carboxylic acid ethyl ester

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