Bis(diethylamino)(dimethylamino)<(triphenylphosphoranyliden)methyl>phosphonium-chlorid

Base Information

Chemical Name:Bis(diethylamino)(dimethylamino)<(triphenylphosphoranyliden)methyl>phosphonium-chlorid
CAS No.:87163-19-7
Molecular Formula:C₂₉H₄₂N₃P₂*Cl
Molecular Weight:530.073
Hs Code.:

Synonyms:Bis(diethylamino)(dimethylamino)<(triphenylphosphoranyliden)methyl>phosphonium-chlorid

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Chemical Property of Bis(diethylamino)(dimethylamino)<(triphenylphosphoranyliden)methyl>phosphonium-chlorid

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Technology Process of Bis(diethylamino)(dimethylamino)<(triphenylphosphoranyliden)methyl>phosphonium-chlorid

There total 4 articles about Bis(diethylamino)(dimethylamino)<(triphenylphosphoranyliden)methyl>phosphonium-chlorid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 87162-93-4
Chlorbis(diethylamino)<(triphenylphosphoranyliden)methylen>phosphoran

: 124-40-3
dimethyl amine

: 87163-19-7
Bis(diethylamino)(dimethylamino)<(triphenylphosphoranyliden)methyl>phosphonium-chlorid

Guidance literature:: In toluene;

Reference yield:

: 685-83-6
bis(diethylamino)chlorophosphine

: 87163-19-7
Bis(diethylamino)(dimethylamino)<(triphenylphosphoranyliden)methyl>phosphonium-chlorid

Guidance literature:: Multi-step reaction with 3 steps

1: 83 percent / toluene / 4 h / Ambient temperature

2: 72 percent / tris(dimethylamino)phosphorane / 1) Ph-Cl, 6 h, r.t., 2) hexane, reflux

3: 83 percent / toluene

With Hexamethylphosphorous triamide; In toluene;

Reference yield:

: 87163-15-3
Chlorbis(diethylamino)phosphonium-chlorid

: 87163-19-7
Bis(diethylamino)(dimethylamino)<(triphenylphosphoranyliden)methyl>phosphonium-chlorid

Guidance literature:: Multi-step reaction with 2 steps

1: 72 percent / tris(dimethylamino)phosphorane / 1) Ph-Cl, 6 h, r.t., 2) hexane, reflux

2: 83 percent / toluene

With Hexamethylphosphorous triamide; In toluene;