1-(2-methyl-3-benzofuryl)-2-(2-methyl-5-phenyl-3-thienyl)perfluorocyclopentene

Base Information

Chemical Name:1-(2-methyl-3-benzofuryl)-2-(2-methyl-5-phenyl-3-thienyl)perfluorocyclopentene
CAS No.:1364381-25-8
Molecular Formula:C₂₅H₁₆F₆OS
Molecular Weight:478.458
Hs Code.:

Synonyms:1-(2-methyl-3-benzofuryl)-2-(2-methyl-5-phenyl-3-thienyl)perfluorocyclopentene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(2-methyl-3-benzofuryl)-2-(2-methyl-5-phenyl-3-thienyl)perfluorocyclopentene

Chemical Property:

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Technology Process of 1-(2-methyl-3-benzofuryl)-2-(2-methyl-5-phenyl-3-thienyl)perfluorocyclopentene

There total 6 articles about 1-(2-methyl-3-benzofuryl)-2-(2-methyl-5-phenyl-3-thienyl)perfluorocyclopentene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 58863-48-2
3-bromo-2-methyl-1-benzofuran

: 308255-22-3
1-[2-methyl-5-phenyl-3-thienyl]heptafluorocyclopentene

: 1364381-25-8
1-(2-methyl-3-benzofuryl)-2-(2-methyl-5-phenyl-3-thienyl)perfluorocyclopentene

Guidance literature:: 3-bromo-2-methyl-1-benzofuran; With n-butyllithium; In tetrahydrofuran; hexane; at -28 ℃; Flow microreactor;

1-[2-methyl-5-phenyl-3-thienyl]heptafluorocyclopentene; In tetrahydrofuran; hexane; at -28 ℃; Flow microreactor;
DOI:10.1002/cssc.201100376

Reference yield:

: 61285-25-4
3-bromo-2-methyl-5-phenylthiophene

: 1364381-25-8
1-(2-methyl-3-benzofuryl)-2-(2-methyl-5-phenyl-3-thienyl)perfluorocyclopentene

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 0 °C / Flow microreactor

1.2: 0 °C / Flow microreactor

2.1: n-butyllithium / tetrahydrofuran; hexane / -28 °C / Flow microreactor

2.2: -28 °C / Flow microreactor

With n-butyllithium; In tetrahydrofuran; hexane;
DOI:10.1002/cssc.201100376

Reference yield:

: 559-40-0
octaperfluorocyclopentene

: 1364381-25-8
1-(2-methyl-3-benzofuryl)-2-(2-methyl-5-phenyl-3-thienyl)perfluorocyclopentene

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 0 °C / Flow microreactor

1.2: 0 °C / Flow microreactor

2.1: n-butyllithium / tetrahydrofuran; hexane / -28 °C / Flow microreactor

2.2: -28 °C / Flow microreactor

With n-butyllithium; In tetrahydrofuran; hexane;
DOI:10.1002/cssc.201100376