N-(8-benzoylaminooctyl)-N,N-bis-[(2-benzyloxy-1-benzyloxymethylethylcarbamoyl)methyl]succinamide

Base Information

Chemical Name:N-(8-benzoylaminooctyl)-N,N-bis-[(2-benzyloxy-1-benzyloxymethylethylcarbamoyl)methyl]succinamide
CAS No.:1333113-82-8
Molecular Formula:C₂₉H₄₇N₅O₉
Molecular Weight:609.72
Hs Code.:

Synonyms:N-(8-benzoylaminooctyl)-N,N-bis-[(2-benzyloxy-1-benzyloxymethylethylcarbamoyl)methyl]succinamide

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Chemical Property of N-(8-benzoylaminooctyl)-N,N-bis-[(2-benzyloxy-1-benzyloxymethylethylcarbamoyl)methyl]succinamide

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Technology Process of N-(8-benzoylaminooctyl)-N,N-bis-[(2-benzyloxy-1-benzyloxymethylethylcarbamoyl)methyl]succinamide

There total 5 articles about N-(8-benzoylaminooctyl)-N,N-bis-[(2-benzyloxy-1-benzyloxymethylethylcarbamoyl)methyl]succinamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1333113-89-5
C₅₇H₇₁N₅O₉

: 1333113-82-8
N-(8-benzoylaminooctyl)-N,N-bis-[(2-benzyloxy-1-benzyloxymethylethylcarbamoyl)methyl]succinamide

Guidance literature:: With 20 % Pd(OH)2/C; hydrogen; In ethanol; at 20 ℃; for 7h;
DOI:10.1016/j.bmcl.2011.06.064

Reference yield:

: 1333113-81-7
N,N-bis[(2-benzyloxy-1-benzyloxymethylethylcarbamoyl)methyl]succinamic acid 2,5-dioxopyrrlidin-1-yl ester

: 1333113-82-8
N-(8-benzoylaminooctyl)-N,N-bis-[(2-benzyloxy-1-benzyloxymethylethylcarbamoyl)methyl]succinamide

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / tetrahydrofuran / 40 h / 20 °C / Inert atmosphere

2: 20 % Pd(OH)2/C; hydrogen / ethanol / 7 h / 20 °C

With 20 % Pd(OH)2/C; hydrogen; triethylamine; In tetrahydrofuran; ethanol;
DOI:10.1016/j.bmcl.2011.06.064

Reference yield:

: 1333113-87-3
C₃₈H₄₅N₃O₆

: 1333113-82-8
N-(8-benzoylaminooctyl)-N,N-bis-[(2-benzyloxy-1-benzyloxymethylethylcarbamoyl)methyl]succinamide

Guidance literature:: Multi-step reaction with 4 steps

1: pyridine / 15 h / 100 °C / Inert atmosphere

2: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / tetrahydrofuran / 18 h / Reflux; Inert atmosphere

3: triethylamine / tetrahydrofuran / 40 h / 20 °C / Inert atmosphere

4: 20 % Pd(OH)2/C; hydrogen / ethanol / 7 h / 20 °C

With pyridine; 20 % Pd(OH)2/C; hydrogen; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In tetrahydrofuran; ethanol;
DOI:10.1016/j.bmcl.2011.06.064