2-chloro-5-fluorobenzoic acid N'-2-fluorophenylhydrazide

Base Information

Chemical Name:2-chloro-5-fluorobenzoic acid N'-2-fluorophenylhydrazide
CAS No.:1358761-75-7
Molecular Formula:C₁₃H₉ClF₂N₂O
Molecular Weight:282.677
Hs Code.:

Synonyms:2-chloro-5-fluorobenzoic acid N'-2-fluorophenylhydrazide

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Chemical Property of 2-chloro-5-fluorobenzoic acid N'-2-fluorophenylhydrazide

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Technology Process of 2-chloro-5-fluorobenzoic acid N'-2-fluorophenylhydrazide

There total 2 articles about 2-chloro-5-fluorobenzoic acid N'-2-fluorophenylhydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 2252-50-8
2-chloro-5-fluoro-benzoic acid

: 2368-80-1
2-fluorophenylhydrazine

: 1358761-75-7
2-chloro-5-fluorobenzoic acid N'-2-fluorophenylhydrazide

Guidance literature:: With dmap; 1-hydroxybenzotriazol-hydrate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 24h;
DOI:10.1039/c1ob05875d

Reference yield: 69.0%

: 2252-50-8
2-chloro-5-fluoro-benzoic acid

: 2924-15-4
(2-fluorophenyl)hydrazine hydrochloride

: 1358761-75-7
2-chloro-5-fluorobenzoic acid N'-2-fluorophenylhydrazide

Guidance literature:: With dmap; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In N,N-dimethyl-formamide; at 20 ℃; for 64h;
DOI:10.1039/c1ob05875d

Reference yield: 58.0%

: 1358761-75-7
2-chloro-5-fluorobenzoic acid N'-2-fluorophenylhydrazide

: 888952-52-1
5-fluoro-1-(2-fluorophenyl)-2,3-dihydro-1H-indazol-3-one

Guidance literature:: With copper(l) iodide; potassium carbonate; L-proline; In dimethyl sulfoxide; at 90 ℃; for 24h; Inert atmosphere;
DOI:10.1039/c1ob05875d