tetra-p-tolyldistibane

Base Information

Chemical Name:tetra-p-tolyldistibane
CAS No.:445401-71-8
Molecular Formula:C₂₈H₂₈Sb₂
Molecular Weight:608.03
Hs Code.:

Synonyms:tetra-p-tolyldistibane

Suppliers and Price of tetra-p-tolyldistibane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of tetra-p-tolyldistibane

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of tetra-p-tolyldistibane

There total 7 articles about tetra-p-tolyldistibane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 31.5%

: 5395-43-7
tri(p-tolyl)antimony

: 445401-71-8
tetra-p-tolyldistibane

Guidance literature:: With Na; BrCH₂CH₂Br; In ammonia; NH3 (liquid); (Ar); p-Tol3Sb was added to soln. of Na in liq. NH3 at -70°C; mixt. was stirred for 1.5 h; BrCH2CH2Br was added dropwise through syringe;mixt. was stirred for 1 h; NH3 evapd.; washed (H2O); dried (vac.); crystd. (Et2O; -23°C); elem. anal.;
DOI:10.1016/S0022-328X(01)01466-8

Reference yield: 26.0%

: 158502-88-6
p-tolylbis(trimethylsilyl)antimony

: 445401-73-0
bis(di-p-tolylantimony)oxide

: (C₆H₄CH₃)2SbOSi(CH₃)3

: [p-tolylantimony]n

: 445401-71-8
tetra-p-tolyldistibane

: 5395-43-7
tri(p-tolyl)antimony

Guidance literature:: With O₂; In tetrahydrofuran; byproducts: ((CH3)3Si)2O; several days in air; other solvent: toluene, mesitylene, 1,4-dioxane andDMF; separation of crystals, washing (petroleum ether); elem. anal.;

Reference yield:

: 871876-14-1
(4-CH₃C₆H₄)2SbI

: 445401-71-8
tetra-p-tolyldistibane

Guidance literature:: With sodium hypophosphite; In ethanol; water; reacting of soln. of Sb compound and aq. ethanolic soln. of NaH2PO2 for 12 h; ppt. washing with aq. ethanol, abs alc., hot xylene and petroleum ether, drying under vac.;
DOI:10.1021/ja01330a056